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GCMS analysis results, sample AD23909, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23909 conducted on October 23, 2001, noting unknown compounds.

NYC-WTC_000067555–000067578

Folder label: “GCMS Scan X 10/2/01 An 10/17/01”

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Scanned page image, NYC-WTC_000067573
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NYC 9/11 Public Portal Document

Librairy Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1801\23909.D Vial: 4 Acq On : 18 Oct 2001 7:07 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.48 1.17 ug/1 109541 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 'entative ID MW MolForm CAS# Qual 1 2-Hexan( 100 C6H12O 000591-78-6 91 2 2-Hex: xjne, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 72 3 Met: Isobutyl Ketone 100 C6H12O 000108-10-1 58 4 Ox»iane, 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 50 Scan 157 (6.480 min): 23909.D (-) m/z 42.95 100.00% 43

5000

nft-> I,,,. ,1.1 20 30 40 50 58

60 71

70 80 90 100

100 110 120 130 140 . L m/z 6.20 6.40 58.05 6.60 6.80 59.28% Abundance #1556:2-Hexanone 43

58 5000 6.40 RTO 6W “m/z 41.00 16.87% 27 I ' I ' ’ ' ' I ’ 71 85 100 ■ I' • ■' I'''' I''' ' I'' ' ' I ‘ ‘ ‘' 1'' ■ ■ I'' • ■ I ■ nfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Mxjndance #11968:2-Hexanone, 4-hydroxy-3-propyk 43

58 ' 6.^ 6.40 6.60 6.80 5000 29 m/z 57.00 13.50%

71 ' I ‘ ‘ ' 1 ■ • ‘ • I I' J. I T’’ 85 100 ,1, ,,,,,, \...I, , , , I , , , ,,, 140 nZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #63354: Methyl Isobutyi Ketone 43 6.20 6.40 6.60 6.80 m/z 100.00 10.63%

L 5000 58

‘I‘‘'1' ‘ I Il 67' I ' ''' t' ' r‘ ‘ 1‘100 j’I‘‘ • I' ' ' ' I ' ‘ ‘ 'I'‘‘‘ I ' A

nZz-> 20 30 40 50 60 70 80 90 100 110 12) 130 140 6.20 6.40 6,60 6.80

23909.D NP101901.M Tue Oct 23 14:32:27 2001 Page 2

NYC-WTC_000067573

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NYC-WTC_000067573Source: NYC Law Department, mirrored locally

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GCMS analysis results, sample AD23910, Oct 2001 · Box DEP Box 60

NYC-WTC_000067579

Gas chromatography-mass spectrometry analysis of sample AD23910 conducted by NYC Department of Environmental Protection labs on October 23, 2001, identifying unknown compounds.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999

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