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GCMS analysis results, sample AD23900, Oct 2001

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DEP lab report for GCMS analysis of sample AD23900 conducted on October 23, 2001, noting unknown compounds.

NYC-WTC_000067453–000067466

Folder label: “GCMS Scan X 10/2/01 An 10/17/01

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NYC 9/11 Public Portal Document

Librairy Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1701\23900.D Vial: 5 Acq On : 17 Oct 2001 5:12 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DAT7mASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2 , R.T. EstConc Area Relative to ISTD R.T. 6.49 0.88 ug/1 78323 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanone / 100 C6H12O 000591-78-6 90 2 Methyl Isobiityl Ketone 100 C6H12O 000108-10-1 53 3 Acetone X 58 C3H6O 000067-64-1 42 4 PentanaX 2-methyl- 100 C6H120 000123-15-9 39 Abundance 7 Scan 158 (6.488 min): 23S00.0 (-) m/z 4X795 100.00% 40

58 5000

85 100 6.20 6.40 660 6.80 ................ . . ,?>lllll 53, I I'l • • • • 71 I ■ I ' I ' ' ' ' 1 ' T m/z 58.05 56.72% nfe-> 10 20 30 40 60 70 80 90 100 Abundance #63384:2-Hexanone 40

_ ....... 5000 58 ' ' 6.^ " 6.^' ‘ 6.60 " 6.^ ' ' ' 29 “mTz 41.05 17705% + I. 71 ' 1‘' ‘ ' I ' 85 ' I ‘ ‘ 100 ' I ' Tlfe-> 10 20 30 40 50 60 70 80 90 100 <\bundance Methyl Isobutyl Ketone 40

6.20 6.40 6.60 6.80 5000 m/z 57.00 13.68% 58

27 85 100 I rV—T- , 67______ I.... I I ‘ ' I ‘ ‘ • • 1 ' ' ' ' I ' ■ ' ' I ‘ T Ti^-> 'io ’ "a,” "ao 40 50 60 70 80 90 100 Abundance #62324: Acetone 40 6.20 6.40 6.60 6.80 m/z 99795 12.55% I 5000 58

15 ■,.,1..,,.i 53 I ' ' ‘ ‘ I ' ‘ ‘ ' I ‘ ‘ ‘ I ' ‘ ‘ ' I ' , I,,, I . 10 20 30 40 50 O) 70 80 90 100 6.20' ' 6.^3 ' ' 6W' ' 6.M '

23900.D NP101901.M Tue Oct 23 12:46:13 2001 Page 2

NYC-WTC_000067462

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NYC-WTC_000067462Source: NYC Law Department, mirrored locally

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