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GCMS analysis results, sample AD23900, Oct 2001

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DEP lab report for GCMS analysis of sample AD23900 conducted on October 23, 2001, noting unknown compounds.

NYC-WTC_000067453–000067466

Folder label: “GCMS Scan X 10/2/01 An 10/17/01

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NYC 9/11 Public Portal Document

Library Search Confound Report Data File : C:\HPCHEM\1\DATA\OCT1701\23900.D Vial: 5 Acq On : 17 Oct 2001 5:12 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Pentanol, 4-methyl- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.74 0.48 ug/1 43143 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanoly^-methyl- 102 C6H14O 000108-11-2 83 2 2-Hexanolz 102 C6H140 000626-93-7 83 3 2-Pentap:ol, 3-methyl- 102 C6H140 000565-60-6 40 4 2-But^ol 74 C4H10O 000078-92-2 39 AbundanceZ Scan 185 (6.736 min): 23900.D (-) m/z 44.95 100.00% 4)5

5000

■ ........... 41 69 6.40 6.60 ’ J ’ ’ ’ ’ I ‘ I ‘ ‘ 6.80 7.00 56 p-rrirl-rTTT 84 87 > I... 1111111■■1111 m/z 69.00 13.88% Tife-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63545:2-Pentanol, 4-methyl- 4)5

i\ [ SaAa 5000 '6.40' 'e.^' e.TO 7.66 m/z 41.0513.20%

nZz-> Mxjndance 20 27

25 30 35 394d,

40 45 57 50 55 60 65 #63583:2-Hexanol a 69

70 75 80 84 85 90 ' I' 95

45

c T T 6.40 6.60 6.80 7.00 5000 m/z 42.95 9.51%

69 ^.58 I 8487 ‘ 1' ■ ■' 1111.1.... I... 11.1.. I.. 111... 11.1.. I.... I. Tife-> 20 25 30 35 40 45 50556065 70 75 80859095 Mxjndance #1777:2-Pentanol, 3-inethyl- 4b 6.40 6.a) 6.80 7.00 m/z 43.95 9.37% 5000

41 56 27 ................ biAr-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 6.40 6.60 6.80 7.00

23900.D NP101901.M Tue Oct 23 12:46:15 2001 Page 3

NYC-WTC_000067463

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NYC-WTC_000067463Source: NYC Law Department, mirrored locally

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