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GCMS analysis results for sample AD24699, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD24699 identifying unknown compounds on November 19, 2001.

NYC-WTC_000068866–000068879

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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NYC 9/11 Public Portal Document

Library Search Confound Report Data File : C:\HPCHEM\1\DATA\NOV0501\24699.D Vial: 18 Acq On : 6 Nov 2001 4:32 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 1.54 ug/1 244919 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 ntative ID MW MolForm CAS# Qual 1 2-Pentanj e, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 53 2 Acetic, Cid, 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 28 3 Acet; e 58 C3H6O 000067-64-1 16 4 Bi ne. 1-ethoxy­ 102 C6H14O 000628-81-9 9 ce Scan 288 (7.691 min): 24699.D (-) m/z 43.00 100.00% 4(3

59 SOM 101 "7.^' ‘7.60 '7.»‘ aro .7 ^.^.,...^1'1 I. 69 S3 _____ I ‘ ‘ I ' ' ‘ ' I ' ' ' ‘ I ' ' ‘ ' I ' ' ' ' I ' mZz 59.05 54.51% TlZz-> 10 20 30 40 60 70 80 90 100 110 Abundance #64275:2-Pentanone. 4-hydroxy-4-methyl- 4(3

5000 59 "7,^' '/to' 7.ro 's.oo'

15 31 101 , , , , ,1, , I , , 83 -r+ ' I ' ' ‘ I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' I ' Tife-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3292: Acetic acid. 1,1-dimethylethyl ester 4(3

7.40 7.60 7.80 8.00 5000 57 m7z 58.05 20.38% 101 15 27 ' I ' ‘ ' 1'''' I' ■ ‘ ‘ 1 ''' ‘ I ■ I 111' '' ' I' tVz-> ' '10 ' ‘ '20' ‘ ‘ 40 50 60 70 80 90 100 110 Abundance #62326: Acetone 4(3 7.^ 7.ro ' 7.80 8.00 m7z 41.05 8.04% 5000 58

+-T-i-j-r-r-r-l-p Tlfe-> 10 20 30 40 50 60 70* " w' ” *90* ” 106 ” 116 7.40 7.60 7.80 8.00

24699.D NP103001.M Tue Nov 13 12:08:10 2001 Page 4

NYC-WTC_000068877

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NYC-WTC_000068877Source: NYC Law Department, mirrored locally

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