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GCMS analysis results for sample AD24699, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD24699 identifying unknown compounds on November 19, 2001.

NYC-WTC_000068866–000068879

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0501\24699.D Vial: 18 Acq On : 6 Nov 2001 4:32 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C_: \HPCHEM\1\METHODS\NP103 001 .M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1,4-Dichlorobenzene-d4 Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.53 ug/1 83983 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentxitive ID MW MolForm CAS# Qual 1 1,4-Dichlor;^enzene-d4 150 C6C12D4 003855-82-1 42 2 Benzene-3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 25 3 Benzenebutanoic acid, 3-nitro-.gamm 223 C10H9NO51 006328-00-3 17 4 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 Shunten^J Scan 711 (11.574 min): 24699.D(-) Tm/z 149.90 100.00%

5000 115 52 rrpT^^trrrfijrTTrp^ '1" I' ■ " I " > 11 ■ I H ( 1111111111. " 11 " " 11 1120 11.40 11.60 11.80 12.00 ra7zJ3T79^^~587T7% TiZz-> 30 40 50 60 70 80 90 1001101201301401501K)1701801902(X)210220 Abundance #9593:1.4-Dichlorobenzene-d4 1$0

5000 115 J 1'^ 11.20 11.40 11.60 11,80 12.00 52 78 m/z 115.00 35.31% 35 JU A 30 40 50 60 70 80 90 100110120130140150160170180190200210220 r Abundance #9592: Benzene-1.2,3,4-d4-, 5,6-dichlora- 1$0

115 11.20 11.40 11.60 11.80 12.00 552 52 78 m/z 78.05 . 19.49%

35 87

TiZz-> I ""1 I A 30 40 50 60 70 80 90 1001101201301401501601701801902002102Z) Abundance #28308: Benzenebutanoic acid, 3-nitro-.gamma.-oxo- 1$0 1120 11.40 11.60 11.80 12.00 m/z 52.00 15731% 5000 104 76 122 134 159 206 223 TmjrrTTpTTqT ■nr n/z-> 30 40 50 60 70 80 so 100110120130140150160170180190200210220 11.20 11.40 11.60 11.80 12.00

24699.D NP103001.M Tue Nov 13 12:08:13 2001 Page 5

NYC-WTC_000068878

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NYC-WTC_000068878Source: NYC Law Department, mirrored locally

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