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GCMS analysis results for sample AD24287, Nov 5 2001

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Laboratory report documenting GCMS analysis of sample AD24287 conducted on November 5, 2001, noting unknown compounds.

NYC-WTC_000068117–000068130

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3101\24238.D vial: 5 Acq On : 31 Oct 2001 8:01 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,4-Dichlorobenzene-d4 Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 11.58 0.52 ug/1 71973 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlorobe: ene-d4 150 C6C12D4 003855-82-1 78 2 Benzene-1,2,3,;X-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 72 3 Benzenebutani c acid, 3-nitro-.gamm 223 C10H9NO5i 006328-00-3 12 4 2-Methyl-6-ly troaniline 152 C7H8N2O2I 000570-24-1 9 Mxindance Scan 711 (11.575 min): 24238.D (-) m/z 149.90 100.00% 1$0

5000 115

52 78 40 I 63 I 87 1120 11.40 11,60 11.80 12.00

TiZz-> T A 30 40 50 60 70 80 90 1001101201301401501601701801902)0210220 m/z 151.90 . 63.01% \bundance #9593:1,4-Dichlorobenzene-d4 Ito

5000 115 78 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 , 40.41% 35 ■pTTT 1‘"'! A 30 40 50 60 70 80 90 100110120130140150160170180190200210220 Abundance #9592: Ben2ene-1,2.3.4-d4-. 5,6-dichloro- 1$0

115 11,20 11.40 11.60 11.80 12.00 5000 52 78 in/z 77.95 . 18.37%

35 87 I I jTTTTp-rrrp-nry I " T nfe-> 30 40 50 60 70 80 90 100110120130140150160170180190200210220 Abundance #28308: Benzenebutanoic acid, 3-nitro-.gamma.-oxo- l40 11.20 11.40 11,60 11.80 12.00 m/z75790 14*87% 5000

56 104 1^ 206 2^ rrrr|TrTTjTTTrjTiTTpTTrpTr^ I ' ' ' 1 ' ' ' O"' “J t pi 1 I I J1 30 40 50 60 70 80 90 100110120130140150160170180190200210220 11.20 11.40 11.60 11.80 12.00

24238.D NP103001.M Pri Nov 02 11:58:52 2001 Page 4

NYC-WTC_000068128

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NYC-WTC_000068128Source: NYC Law Department, mirrored locally

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