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GCMS analysis results for sample AD24429, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting gas chromatography-mass spectrometry analysis of sample AD24429 conducted on November 5, 2001.

NYC-WTC_000068353–000068365

Folder label: “508 GCMS Scan X 10/11/01 An 11/2/01

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Scanned page image, NYC-WTC_000068364
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0201\24429.D Vial: 2 Acq On : 2. Nov 2001 4:02 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 11.58 0.54 ug/1 107272 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlorober[zene-d4 150 C6C12D4 003855-82-1 50 2 Benzene-1,2,^4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 32 3 Benzenebut ^oic acid, 3-nitro-.gamm 223 C10H9NO5i 006328-00-3 17 4 Acenaphtby lene 152 C12H8 000208-96-8 10 Abundance Scan 711 (11.575 min): 24429.D (-) m/z 149.90 100.00% 1$0 I

5000

52 78 115 .... J\... 1120 11.40 11.60 11.80 12.00

TiZz-> 40 I 63 Tyril jnhVr- A i“‘’i 30 40 so 60 70 80 90 100110120130140150160170180190200210220 m7FT^1790~~6j;^ .1 Abundance #9593:1,4-Dichlorobenzene-d4 1$0

5000 115 ..... 52 78 i'i.^' '1'1'40' 'I'tsb' 'I'tso' 'I'zob m7FT147jr~^779^

TiZz-> 35 . .. ||„,7, A T kr^r I '• "I' ‘"I"" I”'' I r 30 40 50 60 70 80 90 100110120130140150160170180190200210220 4bundance #9592: Benzene-1,2,3,4^4-, 5,6-diohloro- 1$0

115 I'i'sp' '11'40' 'iteo 11'so 'izoo 5000 52 78 m7z 78.05 . 22.76%

35 87

Tife-> I P^rt A ik^ 30 40 50 60 70 80 90 1001101201301401501601701801902(X)210220 Abundance #28308: Benzenebutanoic acid, 3-nitro-.gamtna.-oxo- 1$0 11.20 11,40 11.60 11.80 12.00 m7z 52.00 16.25% 5000 104 76

tVz-> Xu. 92 122 134 -[TTTTjtTTTp-tTT 159 206 223 30 40 50 60 70 80 90 10011012013014015016C1170180190 200 210 220 i'iIm '1'1.40 'i?eo 11.so' 12'00

24429.D NP103001.M Mon Nov 05 12:16:01 2001 Page 2

NYC-WTC_000068364

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NYC-WTC_000068364Source: NYC Law Department, mirrored locally

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