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GCMS analysis results for sample AD24474, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24474 conducted on November 9, 2001, identifying unknown compounds.

NYC-WTC_000068460–000068473

Folder label: “GCMS Scan X 10/12/01 An 11/3/01

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Scanned page image, NYC-WTC_000068470
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0201\24474.D Vial: 14 Acq On : 3 Nov 2001 3:41 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 11.57 0.53 ug/1 86196 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 'entative ID MW MolForm CAS# Qual 1 1,4-Dichlc^obenzene-d4 150 C6C12D4 003855-82-1 72 2 Benzene-y2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 40 3 Benzenebutanoic acid, 3-nitro-.gamm 223 C10H9NO5i 006328-00-3 12 4 2-Methyl-6-nitroaniline 152 C7H8N2O2: 000570-24-1 9 Abundance Scan 711 (11.574 min): 24474.D (-) m/z 149.85 100.00% / 1$0

5000 115 78 52 11.20 11.40 11.60 11.80 12.00

■nfe-> A T" ‘ 'T 30 40 50 60 70 80 90 100110120130140150160170180190200210220 4-rTyTTTTpTTTp-rTTp-rTTp^ m/z 151.90 65728% Abundance #9593:1,4-Dichlorobenzene-d4 1$0

5000 52 78 115 .... J\... 11.20 11.40 11.60 11.80 12.00 m/z 114.90 40.36%

■n/z-> 35 ""I ....... A I "'' I 30 40 50 60 70 80 90 100110120130140150160170180190200210220 'I" I" " I" " I" " I" " I ‘' I" " I" " I'

.... J\.. Abundance #9592: Benzene-1.2.3.4-d4-, 5,6-dichloro- 1$0

115 11.20 11.40 11.60 11.80 12.00 5000 52 78 m/z 78.05 23.68% ft 35 87 I -pn-r I TTtAAt p K I'"' I" " I" " I" " I Tife-> 30 40 50 60 70 80 90 100110120130140150160170180190200210220 Abundance #28308: Benzenebutanoic acid, 3-nitro-.gamma.-oxo- 1$0 11.20 11.40 11.60 11.80 12.00 m/z 52.00 14777%

5000

56 104 76 122 134 m/z-> ....... ' I" .. 'I... S..n '' I" “ I'"' I''" I' " 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 220 159 206 223 11.20 11.40 11.60 11.80 12.00

24474.D NP103001.M Tue Nov 13 10:08:07 2001 Page 3

NYC-WTC_000068470

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NYC-WTC_000068470Source: NYC Law Department, mirrored locally

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