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GCMS analysis results for sample AD25038, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD25038 conducted on November 19, 2001, noting violations and unknown compounds.

NYC-WTC_000069215–000069232

Folder label: “GCMS Scan X 10/19/01 An 11/8/01

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Scanned page image, NYC-WTC_000069225
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0801\25038.D Vial: 12 Acq On : 9 Nov 2001 1:21 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T. 11.57 0.52 ug/1 106531 1,4-Dichlorobenzene-d4 11.71

Hit# Of 5 ;ntative ID MW MolForm CAS# Qual

1 l,4-DichlQtobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-X2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 35 3 2-Methox 6-nitroaniline 152 C7H8N2O2 000570-24-1 10 4 Benzal^hyde, 2-hydroxy-3 -methoxy- 152 C8H8O3 000148-53-8 10 Abundance Scan 711 (11.574 min): 25038.D (-) m/z 149.90 .100.00% 150

SY 115 52 78 11.20 11.40 11.60 11.80 12.00

Ti/z-> 20 . ........... 30 40

40 4 50 60 63 70 87 ''I' 80 90 r ' ' ‘ I 1'' '' I 100 110 120 130 140 150 160 m/z 151.90 57.18% Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 115 . ...... . ' ' I ' 78 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 35.44% 35 ' ' I ' ' ' ' I ' ' '' I ®7 ' ' I ' ' ' ' I ' ' h ''' ‘ I' nZz-> 20 30 40 50 60 7080 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-. 5,6-dichloro- ISO

115 11.20 11.40 11.60 11.80 12.00 5000 52 78 m/z 78705 17.69%

35 I ' 11" 11' I '''' I''' • I'' ’ ‘ I'' nfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66883: 2-Methyl-6-nitroaniline 77 1S2 11.20 11.40 11.60 11.80 12.00 m/z 52.00 , 15.30%

5000 106 30 ' I'''' I''' n '' ' ' I ' TTfe-> 20 30 40 50 60 70 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

25038.D NP103001.M Mon Nov 19 12:21:13 2001 Page 3

NYC-WTC_000069225

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NYC-WTC_000069225Source: NYC Law Department, mirrored locally

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