GCMS analysis results for sample AD25038, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0801\25038.D Vial: 12 Acq On : 9 Nov 2001 1:21 am Operator: 209 GALOS Sample ; gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DAT7kBASE\NBS75K.L ********************************************************************* Peak Number 4 1-Monolinoleoylglycerol trimet Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 35.60 0.51 ug/1 114306 Perylene-dl2 37.16 Hit# Of 5 Tentative ID MW MolFoinn CAS# Qual

1 1-Mon^inoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 37 2 Mer^ptoacetic acid, bis (trimethyls 236 C8H20O2SSi2 006398-62-5 12 3 T^s (trimethylsilyl) borate 278 C9H27BO3Si3 004325-85-3 10 4 N‘64ethyladrenaline, tri-TMS 413 C19H39NO3Si3 000000-00-0 9 Abundance Scan 3328 (35.599 min): 25038. D (-) m/z 73.00 100.00% 73

147 5000 221 281 355 43 185 35.20 35.40 35.60 35.80 36.00 112 , , ,L ' I ' ' ' '1 ' ' ' ' I m/z 147.00 61773% ■nZz-> 50 100 150 200 250 300 350 400 450 Abundance #58871:1-Monolinoleoylglycerol tiimethylsilyl ether 7l3

207 / 5000 147 35.20 35.40 35.60 35.80 36.00 34 103 m/z 220.95 40771%

Tlfe-> 1 50 100 I I

150 200 I

250 281

300 350 395 400 450 482

Abundance #30949: Mercaptoacetic acid. bis(trimethylsilyl)- 73 147 I • I I « I I I I I I I . 35.20 35.40 35.60 35.80 36.00 5000 m/z 206.95 22.34% 221 45 193 I. , . 1 104 , 1 T)Zz-> 50 100 150 200 250 300 350 400 450 Abundance #39028: Tris(tnmethylsilyl)borate 73 221 35.20 35.40 35.60 35 80 36,00 m/z 355.05 21.60% 5000 263 133 175 , , I , ,1, , , , , (1,1 , j~t ,k ,1 , I . ........ . , , , I , ■n/z-> 50 100 150 200 250 300 350 400 450 35.20 35.40 35.60 35.80 36.00

25038.D NP103001.M Mon Nov 19 12:21:15 2001 Page 4

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