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GCMS comments for sample AD28157, Nov 2001

Machine-extracted title · confidence 100%

Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.

NYC-WTC_000033800–000033815

Folder label: “GCMS X 11/20/01 A 11/26/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\NOV2601\28157.D Vial: 16 Acq On : 27 NOV 2001 1:22 am Operator: 209 GALOS Sample : 11/20 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************** * * * * ** ************** * * * Peak Number 2 1-Monolinoleoylglycerol trimet Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.

35.58 0.82 ug/1 99702 Perylene-dl2 37.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1 -Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 36 2 1,1,1,5, 77, 7,7-Heptamethyl-3 ,3-bis (t 444 C13H40O5Si6 038147-00-1 12 3 Silana ne, N-[2,6-dimethyl-4- [(tri 281 C14H27NOSi2 072088-09-6 11 4 3-Trim thylsilyloxystearic acid, tr 444 C24H5203Si2 000000-00-0 9 Abundance Scan 3326 (35.578 min): 28157.D (-) m/z 73.00 100.00%

J 73 147

5000 221

‘I r' 1 I 11 ' ' I ' ' TTPfTfir 281 355 327 I 401 429 35.20 35.40 35.60 35.80 36.00 41 112 T—f -- । 185,4 1253. -4—1 + . . | , — m/z 147.00 69.78% m/z—> 50 100 150 200 250 300 350 400 450 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 TI—E—E—mr TIPTIT......... f 35 20 35.40 35.60 35 80 36.00 34 103 m/z 221.05 44.76% — 281 1 1 1 I ■ 1 r1 _... 395 —I———m—TTTTT 482 mlz-> 50 100 150 200 250 300 350 400 450 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73 "T 11 TT 147 35 20 35,40 35,60 35.80 36.00 267 m/z 281.00 25.35% 5000 355 429 45 207

m/z-> LX 50 100 150 ----- 200 250 —

300 350 400 450 Abundance #39584: Silanamine, N-(2,6-dimethyl-4-((trimethyisilyljoxy) TT T it 73 35 20 35.40 35.60 35.80 36.00 281 m/z 354.95 22.30% 209 5000 45 251 179 125 147

m/z—> --------- I 50 100 150 4 200 250 300 350 400 450 TT FT 35.20 35.40 35.60 35.80 36.00

28157.D GCMS1126.M Wed NOV 28 09:13:44 2001 Page 2

NYC-WTC_000033808

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NYC-WTC_000033808Source: NYC Law Department, mirrored locally

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