NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\NOV2601\28157.D Vial: 16
Acq On : 27 NOV 2001 1:22 am Operator: 209 GALOS
Sample : 11/20 scan Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
********************************************** * * * * ** ************** * * *
Peak Number 2 1-Monolinoleoylglycerol trimet Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
35.58 0.82 ug/1 99702 Perylene-dl2 37.12
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1 -Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 36
2 1,1,1,5, 77, 7,7-Heptamethyl-3 ,3-bis (t 444 C13H40O5Si6 038147-00-1 12
3 Silana ne, N-[2,6-dimethyl-4- [(tri 281 C14H27NOSi2 072088-09-6 11
4 3-Trim thylsilyloxystearic acid, tr 444 C24H5203Si2 000000-00-0 9
Abundance Scan 3326 (35.578 min): 28157.D (-) m/z 73.00 100.00%
J
73
147
5000 221
‘I r' 1 I 11 ' ' I ' ' TTPfTfir
281 355
327 I 401 429 35.20 35.40 35.60 35.80 36.00
41 112
T—f -- ।
185,4 1253. -4—1 + . . | , — m/z 147.00 69.78%
m/z—> 50 100 150 200 250 300 350 400 450
Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether
73
207
5000 147 TI—E—E—mr TIPTIT......... f
35 20 35.40 35.60 35 80 36.00
34 103 m/z 221.05 44.76%
— 281
1 1 1 I ■ 1 r1
_... 395
—I———m—TTTTT
482
mlz-> 50 100 150 200 250 300 350 400 450
Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t
73
"T 11 TT
147 35 20 35,40 35,60 35.80 36.00
267
m/z 281.00 25.35%
5000
355 429
45 207
m/z->
LX 50 100 150
-----
200 250
—
300 350 400 450
Abundance #39584: Silanamine, N-(2,6-dimethyl-4-((trimethyisilyljoxy) TT T it
73 35 20 35.40 35.60 35.80 36.00
281 m/z 354.95 22.30%
209
5000
45 251
179
125 147
m/z—>
--------- I
50 100 150
4 200 250 300 350 400 450
TT FT
35.20 35.40 35.60 35.80 36.00
28157.D GCMS1126.M Wed NOV 28 09:13:44 2001 Page 2
NYC-WTC_000033808
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