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GC/MS analysis results for sample AD25047, Nov 27 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD25047 conducted on November 27, 2001.

NYC-WTC_000069323–000069333

Folder label: “GCMS Scan X 10/22/01 An 11/8/01

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Scanned page image, NYC-WTC_000069332
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0801\25047.D Vial: 6 Acq On : 8 Nov 2001 7:30 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 11.58 0.51 ug/1 120996 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Dichlorobenz4ne-d4 150 C6C12D4 003855-82-1 50 2 Benzene-1,2,3,^d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 16 3 2-Methyl-6-niyroaniline 152 C7H8N2O2! 000570-24-1 10 4 Benzaldehyde/ 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 Abundance / Scan 712 (11.579 min): 25047.D (-) m/z 149.90 100.00% Ito

5000 115 52 78 ' I ' ' ' ' I ' ' ' Q ' ' ' ' I ' ' ' ' I ' 11.20 11.40 11.60 11.80 12.00 40 I , 63 I ' I ‘ • I I ' ' ' ' r ' ' 'T' * ' ' I m/z 151.90 62.86% Ti/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1.4-Dichlorobenzene-d4 1$0

5000 115 - 78 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 15717% 35 44^ T)fe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592; Benzene-1,2,3,4-d4-. 5,6-dichloro- 1!0

115 11.20 11.40 11.60 11.80 12.00 fflilil 52 78 m/z 77.95 18.33%

87

Ti/z-> 20 30 35 I 40 50 ' I'' ‘ ' I' 60 70 I ' r ''' r 80 90 100 110 120 A 130 140 150 160 4^ Abundance #66883; 2-Methyl-6-nitroaniline 77 1!!2 11.20 11.40 11.60 11.80 12.00 m/z 52.00 15.23%

5000 106 52

TiZz-> 20 30

30 40 1 50 60 70 80 94

90 100 .. xX.. 110 120 130 140 150 ' ' I ' 160 11.20 11.40 11.60 11.80 12.00

25047.D NP103001.M Mon Nov 19 15:08:29 2001 Page 2

NYC-WTC_000069332

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NYC-WTC_000069332Source: NYC Law Department, mirrored locally

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