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GC/MS analysis results for sample AD25044, Nov 27 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD25044 conducted on November 27, 2001.

NYC-WTC_000069302–000069312

Folder label: “GCMS Scan X 10/22/01 An 11/8/01

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Scanned page image, NYC-WTC_000069311
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0801\25044.D Vial: 5 Acq On : 8 Nov 2001 6:31 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.58 0.53 ug/1 115569 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Dichloro^nzene-d4 150 C6C12D4 003855-82-1 72 2 Benzene-1,2 73,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 12 3 2-Methyl-6yhitroaniline 152 C7H8N2O2i 000570-24-1 10 4 2- Adamant^one_____________________________ 150 C10H14Q 000700-58-3 9 Abundance Scan 712 (11.579 min): 25044.D (-) pm/z 149.90 100.00% Ito

5000 115

52 ... n . S.. 1120 11,40 11.60 11.80 12.00 40 I I I'l I' I I I I ,1 l I I r-i I Il-l |l| I I64 87i’ I I'l' 99 T-YA-r T m/z 151.90 63711% •nZz--> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichloroben2ene-d4 1$0

115 78 11 20 11.40 11.60 11.80 12.00 52 m/z 114.90 39.45%

■Tife-> 20 30 35 40 50 60 JU 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 1120 11'40 Itto 11^0 12'00 115 5000 52 78 m/z 77.95 19714%

87

tt/z-> 20 30 35 40 50 -r-p-r-n-p- 60 70 80 I -rT-p-r-n-f 90 A 100 110 120 130 140 150 160 Abundance #66883: 2-Methyl-6-nitroaniline 77 152 11.20 11.40 11.60 11.80 12.00 m/z 52.00 14.59%

aSE 106 52

Ti/z-> 20 30

30 40 1 T-p-T 50 60 70 80 90 94 122 11 ’ ’ 11' 1111 100 110 120 130 140 150 160 J 11.20 11.40 11.60 11.80 12.00

25044.D NP103001.M Mon Nov 19 15:07:48 2001 Page 2

NYC-WTC_000069311

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NYC-WTC_000069311Source: NYC Law Department, mirrored locally

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