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GCMS analysis results for sample AD24881, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD24881 conducted on November 19, 2001, noting unknown compounds.

NYC-WTC_000069051–000069061

Folder label: “GCMS Scan X 10/18/01 An 11/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOVO 601\24881.D Vial: 12 Acq On : 6 Nov 2001 11:31 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.54 ug/1 104333 1,4-Dichlorobenzene-d4 11.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 l,4-DichlorpDenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-lz^3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 16 3 2-Methyl<^-nitroaniline 152 C7H8N2O2: 000570-24-1 10 4 Benza3?aehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 Abundance Scan 711 (11.571 min): 24881 .D (-) Hm/z 149.90 100.00% 1!0

5000 115

52 78 , I . . , . I . . . rj . , , ,'y 1 . 1 , I . 40 87 11.20 11.40 11.60 11.80 12.00 I ■ " ■ I' ‘ n/z-> 20 30 40 50 60 ' ■ 1 ‘ T rX 70 80 90 100 110 12) 130 140 150 160 m/z 151.90 65.04% ^bundance #9593:1.4-Dichlorobenzene-d4 Ito

5000 115 T J T ' ' 11.20 11.40 11.60 11.80 12.00 52 78 m/z 114.90 38.46%

Ttfe-> M 35 • I • • • • I • > • • 11 > • ■ I ■ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Ji Abundance #9592: Benzene-1,2.3.4-d4-, 5.6^ichloro- liiO T 1 15 11.20 11.40 U.K) 11.80 12.00 5000 52 78 m/z 777^5 19.85%

35 87 I I Ji niZz-> 20 Abundance 30 40 50 60 70 80 90 100 110 120 130 140 150 160 #66883:2-M8thyl-6-nitfoaniIine 77 Ito jj 11.20 11.40 11.60 11.80 12.00 m/z 52.00 . 15.94% 5000 106 52 94 30 i ’Sj^ T ■ I ■ I ■ ■ I ■ • • 1 . I ' ■ I ' I ' TiZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11,60 11,80 12.00

24881.D NP103001.M Fri Nov 16 12:12:07 2001 Page 2

NYC-WTC_000069060

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NYC-WTC_000069060Source: NYC Law Department, mirrored locally

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