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GC/MS analysis results for sample AD23799, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23799 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089311–000089332

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089321
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3001\23799.D Vial: 10 Acq On : 30 Oct 2001 11:19 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1,00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,4-Dichlorobenzene-d4 Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.56 ug/1 145997 1,4-Dichlorobenzene-d4 11.72

Hit# of 5 ;ntative ID MW MdlForm CAS# Qual

1 1,4-Dichl^obenzene-d4 150 C6C12D4 . 003855-82-1 50 2 Benzene-l/f2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 16 3 2-Methyls-nitroaniline 152 C7H8N2O2 000570-24-1 10 4 Benzal^hyde, 2-hydroxy-3-methoxy- 152 C8H803 ■ 000148-53-8 10 Abundance Scan 711 (11.568 min): 23799.D (-) m/z 149.90 100.00% 1 1‘0

5000 115

52 78 ........ ............. 40 11.20 11.40 11.60 11.80 .-rrtUt ''87' I ' 99 m/z 151.90 59.48% ■nZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 (1 Abundance #9593:1,4-Dichlorobenzene-d4 1!i0

5000 115 78 11 20 11.40 11.60 11.80 52 m/z 114.90 40.80% 35 ,,.l „?.......... 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance__ ________ #9592: Benzene-1,2,3.4-d4-. 5,6-dichloro- liiO ....... ............. 115 11 20 11.40 11.60 11.80 5000 52 78 “m/z^ 78.05 20.41%

_ _ __ _ __35_____ ___ ____ 87 . . ... I..... I 11 '■ 1111111,1 ,,,,,,,,,,,,,,,, ' I' 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 <\bundance #66883: 2-Methyl-6-nitroaniline .n , (.......... Xi-— 1$2' .11.20---.11.40-1.1.60 =.11:801 m/z52.00 15.84% 5000 -106- 52 94 30 i ' I' ' '' I '''' I' 17 Ti&-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160: 11.20 11.40 11.60 11.80

23799.D NP103001.M Thu Nov 01 13:16:42'2001^ Page 4

NYC-WTC_000089321

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NYC-WTC_000089321Source: NYC Law Department, mirrored locally

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