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GCMS analysis results for sample AD26130, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26130 conducted on December 3, 2001.

NYC-WTC_000030992–000031002

Folder label: “GCMS X 11/2/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV3001\26130.D Vial: 67 Acq On 1 Dec 2001 7:18 am Operator: 209 GALOS Sample 11/2 gc/ms Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.56 0.59 ug/1 121256 1,4-Dichlorobenzene-d4 11.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 64 2 Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 33 3 Benzenebutanoic acid, 3-nitro- .gamm 223 C10H9NO5i 006328-00-3 17 4 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H803 000148-53-8 10 Abundance Scan 710 (11.560 min): 26130. D (-) m/z 149.90 100.00% 150

5000 115 78 52 11.20 11.40 11.60 11.80 38 JU m/z-> 30 40 50 60 70 80 90 100110120130140150160170180190200210220 ....... P11I.... I.... I. m/z 151.90 61.87% Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 115 TIIm 78 1120 11.40 11.60 11.80 52 m/z 114.90 36.72% 35 87 ‘ 1" mlz-> 30 40 50 60 70 80 90 100110120130140150160170180190200210220 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 —, । i , , , । , TTprr . . । । . । । । . 115 11.20 11.40 11.60 11.80 5000 52 78 m/z 77.95 22.21%

35 87 । I _ TT1——p—nnnummnp—1TrpTE1EEEE1_EEIOIT m/z-> 30 40 50 60 70 80 90 1001101201301401501601701801902X 210220 Abundance #28308: Benzenebutanoic acid, 3-nitro-.gamma.-oxo- 150 11.20 11.40 11.60 11.80 ' m/z 52.00 17.39% 5000 56 104 76 ______ , ,| 92 __ 122 .. 134 1159 206 223 । f । । i i j । i TTTT TIPTIr m/z—> 30 40 50 60 70 80 90 100110120130140150160170180190200210220 11.20 11.40 11.60 11.80

26130.D NP112601.M Mon Dec 03 12:17:37 2001 Page 3

NYC-WTC_000031001

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NYC-WTC_000031001Source: NYC Law Department, mirrored locally

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