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GCMS analysis results for sample AD28263, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report detailing GCMS analysis of sample AD28263 conducted between November 21 and 26, 2001.

NYC-WTC_000034198–000034212

Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2601\28269.D Vial: 24 Acq On : 27 NOV 2001 11:10 am Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Paramss LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,4-Dichlorobenzene-d4 Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 11.56 0.54 ug/1 105811 1,4-Dichlorobenzene-d4 11.70 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlor obenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzenebu noic acid, 3-nitro-.gamm 223 C10H9NO5i 006328-00-3 17 3 Benzene-1 , 2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 12 4 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H803 000148-53-8 10 Abundance 7 Scan 710 (11.561 min): 282®.D (-) m/z 149.90 100.00%! 150

5000 115 52 78 1120 11.40 11.60 11.80 | 38

mlz-> — +63.441+8%. " ।" ■ ■ । a ।।।. J______________ 207 I 111 111 111 11 | 11 H 11. H p .. . |. . . I |. H q . 30 40 50 60 70 80 90 100110120130140150160170180190200210220 m/z 151.90 _ 63.62%| Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 115 78 11.20 11.40 11,60 11.80 | 52 m/z 115.00 _ 37.26%| 87 miz-> 35 I"1' I TnnT 'U''" .।।.irn-np- 30 40 50 60 70 80 90 100110120130140150160170180190200210220 lk.. Abundance #28308: Benzenebutanoic acid, 3-nitro-.gamma.-oxo- 150 . । । i j-T-p-r-r , | TT . .fib . . j , 1120 11,40 11,60 11.80 ! 5000 m/z 78.05 . 19.52%| 56 104 76 | 159 92 122 134 206 223 T m TTTTTTTTTTTT TWTTTTTT I ■ ■ . I ■ . .. I ■ H I | 11. 11 > U ■ I ■ 11 >! < ■ > i I > ■ i < I ■ TpTTTfTT m/z—> 30 40 50 60 70 80 90 100110120130140150160170180190200210220 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 140 11.20 11.40 11.60 11.80...| m/z 52.00 15.81% 115 5000 52 78

m/z—> 35 I "i" "i" "i "11'" ‘ 111 87 I TCTTTTTTTT + * M1 •" j ” < • TTp-rrrpTrrp- 30 40 50 60 70 80 90 100110120130140150160170180190200210220 *T’TT——Tu’TOTT..TT 11.20 11.40 11.60 11.80

28269.D GCMS1126.M Fri Nov 30 13:12:32 2001 Page 1

NYC-WTC_000034205

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NYC-WTC_000034205Source: NYC Law Department, mirrored locally

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