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GCMS analysis results for sample AD23993, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD23993 conducted on October 25, 2001, noting unknown compounds.

NYC-WTC_000067720–000067734

Folder label: “GCMS Scan X 10/4/01 An 10/18/01

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NYC 9/11 Public Portal Document

Library Search Confound Report Data File : C:\HPCHEM\1\DATA\OCT1701\23994.D Vial: 16 Acq On : 18 Oct 2001 3:56 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.75 1.62 ug/1 153688 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative/ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methy1- 116 C6H12O2 000123-42-2 50 2 Acetic acid, l^X-dimethylethyl este 116 C6H12O2 000540-88-5 33 3 Morpholine, /methyl- 101 C5H11NO 000109-02-4 9 4 3-Hydroxy-2/ entanone 102 C5H10O2 003142-66-3 9 \bundance Scan 295 (7.746 min): 23994.D (-) m/z 42.95 100.00% 4t3

59 5CXX)

101 ‘ I > • ' • I ' • • ■ I ■ • • ■ I I 7.40 7.60 7.80 8.00 53., 71 83 ' I ' ‘I I I * ' I ' ' ' ‘ I ‘ ' I ‘ m/z 59.05 51.84% Tife-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64275:2-Pentanone, 4-hyclroxy-4-methyl- 4t3

5000 59 7X0 7.60 7.80 8.00 m/z 100.95 19.45% 15 31 101 I ■ I I, , . . . .. ”... 1 J, , ’ I ' ’ ’ ’ 1 ’ ' ' • 1 * • ‘ ' I ' ' * * I ’ ' ‘ ‘ 1 nfe-> 10 20 30 40 60 70 80 90 100 110 Abundance #3292: Acetic acid, 1,1 -dimethylethyl ester 4(3 T-T-p-m-r-TT-H-r T*' “t I ■ ■ ■ ■ I ■ 7.40 7.60 7.80 8.(X) 5000 57 m/z 58.05 17.60% 101 27 ' ' ' I ' ‘ I * ‘ ' I ’ ’ ’ ‘ I • ' I ' ‘ ' I ' ' ' ‘ I T)fe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1640: Morpholine, 4-tn8thyl- ■ I I ' " . I ■ ■ f 4(3 7.40 7.60 7.80 8.00 m/z 41.05 7704% 5000 101 15 71 I r-j—n-'-r-r—p -+W- 27 I 56 I > ■ 1 I I I IT' p--r-r-rT-|--r-r-r-r-p-r-r-r-p- inZz-> 10 20 30 40 50 70 80 90 100 110 7.40 7.60 7.80 8.00

23994.D NP101901.M Wed Oct 24 11:24:48 2001 Page 5

NYC-WTC_000067732

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NYC-WTC_000067732Source: NYC Law Department, mirrored locally

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