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GCMS analysis results for sample AD23993, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD23993 conducted on October 25, 2001, noting unknown compounds.

NYC-WTC_000067720–000067734

Folder label: “GCMS Scan X 10/4/01 An 10/18/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1701\23994.D Vial: 16 Acq On : 18 Oct 2001 3:56 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplrs 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 1,4-Dichlorobenzene-d4 Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 11.62 0.51 ug/1 48372 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 l,4-Dichloro^^zene-d4 150 C6C12D4 003855-82-1 95 2 Benzene-l,2<3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 53 3 Benzofur^fltb 7-chloro- 152 C8H5C1O 024410-55-7 9 4 Benz enamine, 2-methyl-4-nitro-152 C7H8N2O2 ____ 000099-52-5 7 Wjundance Scan 717 (11.620 min): 23994.D (-) m/z 149.90 100.00% 1!i0

5000 115 52 78 40 11.20 11.40 11.60 11.80 12.00 ■■ ■m7z~T5T75^ 60.29% nZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 <\bundance #9593:1,4-Dichlorobenzene^4 1!i0

5000 115 I ■ , . . 1 . .. I p 1 f., , I .,

78 11.^ 11.40 11.60 11.80 12.00 52 m/z 114.90 40730% 35 87 t,fe-> 30 40 50 60 70 80 90 100 110 W 130 150 160 \bundance #9592: Benzene-1.2.3.4-d4-. 5,6-<iichloro- liW

115 11.20 11.40 11.60 11.80 12.00 5000 52 78 "mTz 78.05 20.30%

35 87 I I ' 1 ‘‘ 1'''' I'''' 1' 11 ■ • ■ ■ 11 T Tife-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10136: Benzofuran, 7-chloro- 1!12 11.20 11.40 11.60 11,80 12.00 “m/z 5270^ 19.38% 5000 89

63 35 73 125 ■pm-r-p-n-r ' ‘ 1 ‘ T Tife-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

23994.D NP101901.M Wed Oct 24 11:24:50 2001 Page 6

NYC-WTC_000067733

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NYC-WTC_000067733Source: NYC Law Department, mirrored locally

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