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GC/MS analysis results for sample AD22752, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22752 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087379–000087389

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File ; C;\HPCHEM\l\DATA\SEP2801\22752.D Vial: 17 Acq On : 29 Sep 2001 4:07 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,4-Dichlorobenzene-d4 Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 11.65 0.52 ug/1 67630 1,4-Dichlorobenzene-d4 11.79 Hit# Of 5 Tentative ID MW MolForm CAS# Qua!

1 1,4-DiZhlorobenzene-d4 150 C6C12D4 003855-82-1 64 2 Benz ^e-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 43 3 Bena41dehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 14 4 Be^ enamine, N-methyl-4-nitro- 152 C7H8N2O2i _______000100-15-2 14 ^bundany Scan 720 (11,647 min): 22752,0 (-) m/z 149.90 100.00% 1!i0

222

40 52 78 115 is 11,40 11,60 11,80 12,00 •

Tife-> 30 40 50 63 60 ..... J,.”,......... 70 80 90 100 110 120 130 140 150 160 m/z 151.90 59.88% Abundance #9593:1,4-Dichlorobenzene-d4 1!i0

222 115 78 11,40 11,60 11,80 12,00 52 m/z 115.00 . 36.25% 35 m/z-> 30 40 50 60 . 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 1!i0

115 11,40 11,60 11,80 12,00 5000 52 78 in/z 77.95 . 18.65%

35 87 I ■ p-n-n-p I mZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- 152 L 11,40 11,60 11,80 12,00 m/z 52.00 18733% 106 5000 53 81

122 136 iI -rp-T-n-pr-r-n-j- nnfe-> 30 40 50 60 70 80 100 110 120 130 140 150 160 11.40 11.60 11,80 12,00

22752.D NP091101.M Fri Oct 05 10:29:51 2001 Page 1 NYC-WTC_000087388

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NYC-WTC_000087388Source: NYC Law Department, mirrored locally

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