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GCMS analysis results for sample AD24401, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting gas chromatography-mass spectrometry analysis of sample AD24401 conducted on November 5, 2001.

NYC-WTC_000068336–000068352

Folder label: “508 GCMS Scan X 10/11/01 An 11/2/01

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Scanned page image, NYC-WTC_000068344
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0201\24401.D Vial: 7 Acq On : 2 Nov 2001 8:53 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.51 ug/1 69147 1,4-Dichlorobenzene-d4 11.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlor^enzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-l,^3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 35 3 Acenaphth^ene 152 C12H8 000208-96-8 14 4 Benzenap&ne, 2-methyl-5-nitro- 152 C7H8N2O2 000099-55-8 14 ^bundance / Scan 711 (11.574 min): 24401 .D (-) m/z 149.90 100.00% 1!i0

5000 115 52 78 T-p- , . ■ I nr-, TT ■ ’ ' 1 ‘ 1120 11.40 11,60 11.80 12.00 m/z 151.90 . 66.00% T,fe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 liiO

5000 115 78 1120 11.40 11.60 11.80 12.00 52 m/z 114.90 37779% 35 ■nfe-> 30 " '-w" ’ 50 isb' 70 80 90 100 110 120 130 140 150 160 Abundance #9592: B8nzene-1.2.3.4-d4-. 5.6-diohloro- 1$0 ■ I' ■ " r' ■ ' ‘ ‘ I ' 115 11.20 11.40 11.60 11.80 12.00 5000 52 78 m/z 77795 19.14%

Tl/Z-> Abundance "30 35 I '40' ' ' '50 TT-n-rn-p 60 70 87 I * 1'''' r 80 90 T 100 110 120 130 140 150 160 #67015: Acenaphthylene 1i!2 __L T T 11.20 11.40 11.60 11.80 12.00 in/z 52.00 15.61% 5000

76 126 h 30 40 50 60 70 80 90 100 110 120 130 140 150 160 l‘l.2o' 'l‘l!^' 'l7^ 'll!8b' ‘izoo

24401.D NP103001.M Mon Nov 05 12:22:28 2001 Page 2

NYC-WTC_000068344

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NYC-WTC_000068344Source: NYC Law Department, mirrored locally

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