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GCMS analysis results for sample AD24945, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24945 conducted on November 19, 2001, noting unknown compounds.

NYC-WTC_000069073–000069083

Folder label: “GCMS Scan X 10/18/01 An 11/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0601\24945.D Vial: 13 Acq On : 7 Nov 2001 12:29 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.55 ug/1 109214 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Dichlorobenz/ne-d4 150 C6C12D4 003855-82-1 53 2 Benzene-l,2,3,4/d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 12 3 JP 60 / 151 C10H17N 013074-39-0 9 4 Benzoic acid, 5-dimethyl-________ 150 C9H10O2 000610-72-0 9 iMsundance / Scan 711 (11.572 min): 24945.D (-) m/z 149.90 ,100.00% ii»

5000 115

52 78 ' I' " ■ I " ' ‘ 1 ’

87 11.20 11.40 11.60 11.80 12.00 ■A. I m/z 151.90 65799% nZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 1!i0

5000 115 78 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 38.63% 35 I ' '' ' 1 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benz8n8-1,2,3.4-d4-, 5.6-dichloro- li® . I I I I . I . . . p) . . . . . , . , ,

115 1120 11.40 11.60 11.80 12.00 5000 52 78 m/z 78.05 2^774%

35 87

•nfe-> 30 I 40 mot"' 70 I I'' ‘' 1' 80 90 A 100 110 120 130 1 ’ ' ‘ ‘ 1 140 150 160 ^bucKiance #10046: JP 60 1!» 11.20 11.40 11.60 11.80 12.00 92 56 m/z 52.00 15.90% 79 134 5000

67 108 119 ' I • ■' ‘ I'' •' I • P-lli.. J| .. TT-p-r ' ‘ I ' T-p-n-r-pr-r ' 1 ’ ■nlz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

24945.D NP103001.M Mon Nov 19 11:53:59 2001 Page 2

NYC-WTC_000069082

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NYC-WTC_000069082Source: NYC Law Department, mirrored locally

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