GCMS analysis results, sample AD24399, November 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; Cs\HPCHEM\1\DATA\NOV0201\24399.D Vial: 5 Acq On : 2 Nov 2001 6:57 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 l,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.58 0.53 ug/1 77168 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 'entative ID MW MolForm CAS# Qual 1 1,4-Dichlprobenzene-d4 150 C6C12D4 003855-82-1 90 2 Benzene-/,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 47 3 JP 60 151 C10H17N 013074-39-0 9 4 Benzoi acid, 2,5-dimethyl- 150 C9H10O2 000610-72-0 9 Abundance ? Scan 712 (11.578 min): 24399.D (-) m/z 149.90 100.00% 1!i0

5000 115 52 78 .......... r, J . , 38 11.20 11.40 11.60 11.80 12.00 UpU+tT-rrn-H ....... m/z 151.90 66.13% Tife-> 30 40 50 60 70 80 90 100 110 120 130 140 ISO 160 Abundance #9593:1,4-Dichlorob8nzene-d4 1!i0

5000 115 78 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 38777% 35 87 I ‘ ‘ ' I Ti/z-> "30 " 4o' 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3.4-d4-, 5,6-dictiloro- IliO —I I I I I I ■ I I I II % I I p I I I I I 1

115 11.20 11.40 11.60 11.80 12.00 5000 52 78 m/z 52.00 , 19.43%

87

■n/z-> 30 35 I 40 50 ' I' 60 I ■ I'''' I'''' I' 70 80 90 100 110 A 120 130 140 150 160 Abundance #10046: JP 60 liiO J 11.20 11.40 11.60 11.80 12.00 ‘ ' 1 ‘ 92 56 m/z 78.05 . 17.77% 79 134 553

.JU, 67 108 119

Tl/z-> 30 40 50 60 70 80 90 Ur X ‘ • 1 ‘ 110 120 130 140 150 160 100 n ‘ 11.20 11.40 11.60 11.80 12.00 r T

24399.D NP103001.M Mon Nov 05 12:15:05 2001 Page 2

NYC-WTC_000068323