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GC/MS analysis results for sample AD23839, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23839 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089366–000089384

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089375
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT3001\23839.D Vial: 13 Acq On : 31 Oct 2001 2:14 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M . (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.56 ug/1 144313 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Dichlor>2ibenzene-d4 150 C6C12D4 003855-82-1 94 2 Benzene-ly<2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 38 3 Acenaph^ylene 152 C12H8 000208-96-8 10 4 Benzor^rile, 2-amino-5 -chloro- 152 C7H5C1N2 005922-60-1 9 Abundance7 Scan 711 (11.569 min): 23839.D (-) m/z 149.90 100.00% 1!i0

5000- 115 52 78 f'' ’ ' I’ 38 11 20 11.40 11.60 11.80 , , 62 99 - 1^- m/z 151.90 66783% TiZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11 Abundance #9593:1,4-Dichlorobenzene-d4 1!i0

5000 115 78 11 20 11 40 11.60 11.80 52 m/msToT 38.16% 30 35 40 50 60 JU/ 70 80 90 100 tX 110 120 130 140 I'l'i.... .....150 160 ’ ^Mjundance £9592:Benzene-1,2,3,4-d4-, 5,6-dichloro- i$d

115 11 20 11.40 11.60 11.80 5000 52 78 “m/z 78.05 21.93%

35 . • 4-A. ,, .~7 J,. ,'77T77 ' I'''' I' TiZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #67015: Acenaphthylene ■152 -- m7z 52700 18.58% 5000

76 63 I 126 ■ I |,- 98 "l^ T nZz-> 30 40 50 60 70 80 90 100 110 120I 130 140 150 ■ 11.20 11.40 11.60 11.80

23839.D NP103001.M Thu Nov 01 14:35:55 2001 Page 3

NYC-WTC_000089375

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NYC-WTC_000089375Source: NYC Law Department, mirrored locally

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