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GCMS analysis results for sample AD24401, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting gas chromatography-mass spectrometry analysis of sample AD24401 conducted on November 5, 2001.

NYC-WTC_000068336–000068352

Folder label: “508 GCMS Scan X 10/11/01 An 11/2/01

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Scanned page image, NYC-WTC_000068343
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0201\24401.D Vial: 7 Acq On : 2 Nov 2001 8:53 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Acetic acid, 1,1-dimethylethyl Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.70 0.76 ug/1 103431 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 TentatjjB^e ID MW MolForm CAS# Qual 1 Acetic acid, 1,1<dimethylethyl este 116 C6H12O2 000540-88-5 38 2 2-Pentanone, hydroxy-4-methyl- 116 C6H12O2 000123-42-2 36 3 3-Hydroxy-2^ lentanone 102 C5H10O2 003142-66-3 23 4 Acetone / 58 C3H6O 000067-64-1 9 Abundance A Scan 289 (7.700 min): 24401 .D (-) m/z 42.95 100.00% 4t3

5000 59

101 7.40 zro' ‘7.^' 8.00 ..... • I • • ■ ■ I ■ I I m/z 59.05 48.66% Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64325: Acetic acid, 1.1-dimethylethyl ester 4)3

57 5000 ' '7.^ '7.^' 7.^ 's.oo' ' 101 m7z“T0079r^ 23737% ' ■ '50' ' ^1 'T' ' ' ' I ' ‘ ‘ ' I ' ' ' ”’1 ' ' ' ' 1 I ' ■ ■ ( ' nZz-> 10 20 30 40 60 70 80 90 100 110 Abundance #64275:2-Pentanone, 4-hydroxy-4-methyl- 43 7.^ 7.60 7.80 8.00 5000 m/z 58.05 18.27% 59

15 31 101 I I I rT+ l| , , , , I , , , , I??, , I , I |l, , , , I , T\fz-> 10 20 30 40 ”5" 60 70 80 90 100 110 Abundance #1691:3-Hydroxy-2-pentanone 31 5? 7.40 7.60 7.80 8.00 ■m/z 40795 8734% 5000 45 15 I ...7...^ .. I 1 ' ' ' ' I ' ' ‘ ‘ I ' ' ' ‘ I ' ' ‘ ' I ' , 66 73 84 1 ' * ’ ' I’ ' ‘ ‘ I ' * ‘ ’ I ' 102 T I >•■ ■ ■ I I 10 20 30 40 50 60 70 80 90 100 110

24401.D NP103001.M Mon Nov 05 12:22:26 2001 Page 1

NYC-WTC_000068343

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NYC-WTC_000068343Source: NYC Law Department, mirrored locally

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