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GCMS analysis results for sample AD24134, Oct 29 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24134 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067922–000067935

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT2501\24134.D vial: 15 Acq On : 26 Oct 2001 2:22 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M {RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.60 0.54 ug/1 85985 1,4-Dichlorobenzene-d4 11.73 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 l,4-DichlorQbenzene-d4 150 C6C12D4 003855-82-1 37 2 Benzene-l^/2\3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 25 3 Benzofin^dn, 7-chloro- 152 C8H5C1O 024410-55-7 9 4 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 9 Abundance < Scan 714 (11.595 min): 24134.D (-) m/z 149.90 100.00% 1!i0

5000- 115 78 52 p ' ‘ 1 ‘ I ' ' 11.20 11.40 11.60 11.80 12.00 lff ri I I II I j', l I I 66 l-i [-r-rl 40 .II m/z 151.90 61.74% Tife-> 30 40 50 60 ■70 80 90 100 110 120 130 140 150 160 ft ^bundance #9593:1,4-Dichlorobenzene-d4 liiO

5000 52 78 115 I ‘ H * ' 1 11.^ 11.40 11.60 11.80 12.00 m/z 115.00 39774% 35 87 ■nZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-. 5.6-dfchloro- 1!!0 T 115 11.^ 11.40 11.60 11.80 12.00 5000 52 78 m/z 78705~~2yr8^

35 87 I I 11 •'' * I' A I''' I TiZz-> 'Abundance 30 40 50 60 70 80 90 100 110 120 130 140 150 1«) #10136: Benzofuran, 7-chloro- 15 2 u ’ ' 1 11.20 11.40 11.60 11.80 12.00 m/z 52.00 , 14.39% 5000 89

63 35 49 125 m/z-> 30 40 M 60 70 M 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

24134.D NP101901.M Mon Oct 29 09:33:55 2001 Page 5

NYC-WTC_000067934

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NYC-WTC_000067934Source: NYC Law Department, mirrored locally

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