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← Document results/DEP Box 60/508 GCMS Scan X 10/11/01 An 11/2/01
Document / 11 pages

GCMS analysis results for sample AD24396, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of environmental sample AD24396 with detection of unknown compounds.

NYC-WTC_000068281–000068291

Folder label: “508 GCMS Scan X 10/11/01 An 11/2/01

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Scanned page image, NYC-WTC_000068289
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Confound Report Data File : Cs\HPCHEM\l\DATA\NOV0101\24396.D Vial: 13 Acq On : 2 Nov 2001 2:45 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 0.78 ug/1 103126 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanoney4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 39 2 3-Hydroxy-^pentanone 102 C5H10O2 003142-66-3 9 3 Butane / 58 C4H10 000106-97-8 9 4 Morpholine, 4-methyl-_________ 101 C5H11N0 000109-02-4 9 (Abundance Scan 289 (7.634 min): 24396.D (-) 4t3 m/z 42.95 100.00%

5000 59

101 T ' 7.^ 7.60 7.80 8.00 I I ‘'I'‘'I' ' ' ' I ' ‘ ‘ 'I' fl? I ' ' ‘ ' I ' ' ' ' p’' ' ' p ' ' ‘ 1 ■ ' ' ' I m/z 59.05 49.51% Tl&-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3245:2-Pentanone, 4-hydroxy-4-methyl- 4(3

5000 59 7.40 7.60 7.80 8.00 m/z 100.95 21.83%

L 31 .................................... I I T-r-r+ nfe-> ' ' 'lb' ' ' ' '30' ' 40 50 60 70 80 90 100 110 Abundance #1691:3-Hydroxy-2-pentanone ah 53

7.40 7.60 7.80 8.00 5000 m/z 58765 17.56% 45 15 I , 66 73 84 102 I I • ■ ■ • I ■ • • • I • • • ■ I • ■ • ■ I ■ ■ ■ ' I TiZz-> 10 20 ' I ‘ 30 ' I ‘ 40 ‘ ' I ' 50 60 70 80 90 100 110 -^'■-1- ■■pl' \bundanc8 #99: Butane 43 7.40 7.60 7.80 8.00 m/z 41.00 7.91% 5000

infe-> 10 15

20 29

30 40 58 I ■ ■ I ■ ■ "’I I ■ • • ■ I ■ ■ ■ ■ I • • • • I • • ■ ■ 1 • ■ ■ • I 50 S) 70 80 90 100 110 7.^ k Zro' 7.M 8.00

24396.D NP103001.M Wed Nov 07 14:41:12 2001 Page 1

NYC-WTC_000068289

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NYC-WTC_000068289Source: NYC Law Department, mirrored locally

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