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← Document results/DEP Box 60/508 GCMS Scan X 10/11/01 An 11/2/01
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GCMS analysis results for sample AD24396, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of environmental sample AD24396 with detection of unknown compounds.

NYC-WTC_000068281–000068291

Folder label: “508 GCMS Scan X 10/11/01 An 11/2/01

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Scanned page image, NYC-WTC_000068290
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0101\24396.D Vial: 13 Acq On : 2 Nov 2001 2:45 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.58 0.51 ug/1 68026 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 T .tative ID MW MolForm CAS# Qual 1 1,4-Dichlo: ienzene-d4 150 C6C12D4 003855-82-1 47 2 Benzene-1 ,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 33 3 2-Adaman —one 150 C10H14O 000700-58-3 23 4 Benzo [b .hiophene-4-ol__________ 150 C8H6OS 003610-02-4 9 Abundance Scan 712 (11.578 min): 24396.D (-) m/z 149.90 100.00% 1ii0 ft 5000 115

52 78 ■ I ' ' " I " ' Q 43 ........................ 87 11.20 11.40 11.60 11.80 12.00 '"I'"I I''' '' I' 1'''' I 4^ m/z 151.90 . 63.68% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-<i4 1$0

5000 115 I ‘ ‘‘ I

78 11.20 11.40 U.K) 11.80 12.00 52 m/z 114.90 . 41.16% 35 I'''' 1 ' ‘ I ' m/z-> "30" ' 40''' M 60 70 80 90 100 110 120 130 140 IK) 160 Abundance #9592: Benzene-1,2,3.4-d4-, 5,6-dichloro- 1$0 ' I ' ' ' ' I ‘ ' I ' ' 115 11.20 11.40 11.60 11.80 12.00 5000 52 78 m/z 77795 17.79%

35 I ' I'''' I ‘ I • • •' I • ‘ ‘' I * * * * I'' nnZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 IK) Abundance #9842:2-Adamantanone 1!i0 11;^' 1'1'46' 11 .OT i tro izob m/z sy/oT 16.38% 79 5000-

93 104 117 II 132 ......... I......... ‘ I ‘ ' nnZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11,40 11.60 11.80 12.00

24396.D NP103001.M Wed Nov 07 14:41:14 2001 Page 2

NYC-WTC_000068290

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NYC-WTC_000068290Source: NYC Law Department, mirrored locally

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