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GCMS analysis results for sample AD24730, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24730 identifying unknown compounds on November 19, 2001.

NYC-WTC_000068893–000068906

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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Scanned page image, NYC-WTC_000068905
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0501\24730.D Vial: 20 Acq On : 6 Nov 2001 6:29 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 5 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.55 ug/1 100924 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Teiifeative ID MW MolForm CAS# Qual 1 l,4-Dichlo3?6benzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene;>a<2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 32 3 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 4 4-Aotino-2-chlorobenzonitrile _______ 152 C7H5C1N2 020925-27-3 9 'Abundance Scan 711 (11.572 min): 24730.D (-) Tm/z 149.90 100.00% 1!i0

A 5000 115 52 78 40 11.20 11.40 11.60 11.80 1Z00 ' I ' ‘ ' I I. ■. 1111111.. m/z 151.90 61.25% Ti/z-> Abundance 30 40 50 60 70 80 90 100 110 120 130 #9593:1.4-Dichlorobenzene-d4 140 150 160 J 1!O

5000 115 78 11.20 11.40 11.60 11,80 12.00 52 m/z 114.90 36.90% 35 1 ' ‘ ‘ ' 1 ■n&-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-44-, 5,6-dichloro- 1$0 , I Q , ‘ .... I ■ 115 11.20 11.40 11.60 11.80 12.00 5000 52 78 m/z 77795 20.00%

87

n&-> 30 35 ' I'''' I' ■'' 1 40 50 ''' 1'''' I'' 60 70 80 I I' ‘ ‘' 1' 90 100 110 120 130 A 140 150 160 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- 142 JX—T- 11.^ 11'40' 11.TO ‘I'iJO 1Z00 m/z 52.00 16.28% 106 5000 53 81

Tife-> 30 40 50 60 70 K) 90 92 ...III.. .......... i I 100 110 120 130 140 150 160 ■ I ■ I ■ . I . ■, i~] ■ • ./Y' I '' 1 ‘ 1120 1140 1160 1180 1200

24730.D NP103001.M Tue Nov 13 12:11:51 2001 Page 5

NYC-WTC_000068905

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NYC-WTC_000068905Source: NYC Law Department, mirrored locally

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