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GCMS analysis results for sample AD24052, Oct 29 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24052 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067894–000067907

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT2501\24052.D Vial: 13 Acq On : 26 Oct 2001 12:25 am Operator: 209 GALOS Sample : gc/ms unknovzn Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L

Peak Number .5 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.59 0.55 ug/1 104331 1,4-Dichlorobenzene-d4 11.74 Hit# of 5 Temtative ID MW MolForm CAS# Qual 1 l,4-Dichlo»6benzene-d4 150 C6C12D4 003855-82-1 95 2 Benzene-]^, 3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 50 3 Benzald^yde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 25 4 Acenaptufhylene_________ _________________ 152 C12H8 000208-96-8 9 Abundance y Scan 713 (11.593 min): 24052.D (-) m/z 149.90 100.00% ii»

5000 115 52 78 T 40 11.^ 11.40 11.60 11.80 12.00 m/z 151.90 61.45% nfe-> ^bundance 30 40 50 60 70 80 90 100 110 120 130 140 150 160 #9593:1,4-Dichlorobenzene-d4 1$0 A 5000 115 78 11.^ 11.40 11.60 11.80 12.00 52 m/z 114.90 42.00% 87 TiZz-> 30 35 40 ' I ‘‘' I'''' I' 50 60 70 80 90 100 110 120 130 140 150 160 flu. <Mxjndance #9592: Benzene-1,2,3,4-d4-, 5.6-dichloro- 1$0 T 115 11.20 11.40 11.60 11.80 12.00 5000 52 78 m/z 52.00 21.63%

35 I ' I '' ‘ I'''' I'' I' 7... „lii.... Ti/z-> M40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- 1$2 11.^ 11.40 11.60 11.80 12.00 m/z 78.05 20.25% 106 5000 53 81

122 ‘ I ‘' 1'''' I' 92 A- 136 I I T 'nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11,20 11.40 11.60 11.80 12.00

24052.D NP101901.M Fri Oct 26 10:32:41 2001 Page 5

NYC-WTC_000067906

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NYC-WTC_000067906Source: NYC Law Department, mirrored locally

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