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GC/MS analysis results for sample AD23359, Oct 19 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23359 conducted on October 19, 2001.

NYC-WTC_000088636–000088647

Folder label: “GC/MS Scan 9/26/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT1801\23359.D Vial: 8 Acq On : 18 Oct 2001 11:02 pm Operator: 209 GALOS Sample : gc/ms unknown re extracted Inst ; GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 11.63 0.50 ug/1 47373 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Tentative ID MW MolForm CAS# Qnal

1 l,4-Dichlorob6nzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-1,2/3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 25 3 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 4 Acenaphth/lene 152 C12H8 000208-96-8 9 Abundance Scan 717 (11.627 min): 23359.D (-) m/z 150.00 100.00% 1!i0

5000 115 78 52 11.20 11.40 11.60 11.80 12.00 40 TiL+rTT I ....... m/z 151.90 69.10% mfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 1ii0

5000- 115 78 11.20 11.40 11.60 11.80 12.00 52 m/z 115.00 34.78% 35 .■,.,.,,1,1,,,,,,,,^ ! mfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 1$0

115 11.20 11,40 11,60 11.80 12.00 5000 52 78 m/z 78.05 21.96%

35 87 I ' I ' ' '' I ' ' ' ' I' I tJJ't m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- 1!i2 11.20 11.40 11.60 11.80 12.00 "mTz 527 0 0 1 6789% 106 553 53 81

122 136 I. •n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

23359.D NP091101.M Fri Oct 19 10:14:49 2001 Page 3

NYC-WTC_000088646

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NYC-WTC_000088646Source: NYC Law Department, mirrored locally

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