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GCMS analysis results for sample AD23997, Oct 29 2001

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Laboratory report documenting GCMS analysis of sample AD23997 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067782–000067795

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT2501\23997.D Vial: 5 Acq On : 25 Oct 2001 4:36 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.60 0.55 ug/1 106748 1,4-Dichlorobenzene-d4 11.73 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 l,4-DichlorobenXene-d4 150 C6C12D4 003855-82-1 64 2 Benzene-1,2, ^-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 43 3 Benzaldehyde^^ 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 4 Acenaphthylene 152 C12H8 000208-96-8 9 Abundance 7 Scan 714 (11.597 min): 23997.D (-) m/z 149.90 100.00% liiO

5000 115 52 78 I''' ‘ 1 T 11.^ 11.40 11.60 11.80 12.00

30 40 40 50 60 63 70 I 80 87 90 77 100 110 120 130 140 150 160 m/z 151.90 60795% Abundance #9593:1,4-Dichlorobenzene-d4 1iO

5000 115 T T 78 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 35.58%

ttZz-> 30 35 40 50 87 -pT-rr- 60 70 80 90 100 110 120 130 140 150 1«) 3. I'''' I ■■

Abundance #9592: Benzene-1,2.3.4-d4-, 5,6-dichloro- liiO T 115 11.20 11.40 11.60 11.80 12.00 5000 52 78 m/z 78.05 19.21%

35 I 4^ nZz-> Abundance "30" ‘ 40''' 50 ' I' 60 70 80 90 100 110 120 130 140 150 160 #66892: Benzaldehyde. 2-hydroxy-3-methoxy- 1ii2 T R T 11.20 11.40 11.60 11.80 12.00 m/z 52.00 18.31% 106 5000 53 81

nZz-> 30 40 50 60 70 130 --th 90 92 122 j| 136 p-TTTYt-r-r-ryTT-TTTTn-T^ 100 110 120 130 140 150 160 I I R 11.20 11.40 11.60 11.80 12.00

23997.D NP101901.M Fri Oct 26 10:11:03 2001 Page 5

NYC-WTC_000067794

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NYC-WTC_000067794Source: NYC Law Department, mirrored locally

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