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GC/MS analysis results for sample AD23124, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23124 conducted on October 12, 2001.

NYC-WTC_000088000–000088022

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088009
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NYC 9/11 Public Portal Document

Library Search Compound Report'

Data File C:\HPCHEM\1\DATA\OCT0401\23124.D Vial: 12 Acq On 5 Oct 2001 2:18 am Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise -Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

11.64 0.55 ug/1 93239 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 l,4-Dichlo/obenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-l/2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 43 3 Benzald^yde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 4 4-Amin0^2-chlorobenzonitrile 152 C7H5C1N2 020925-27-3 9 Abundance Scan 719 (11.639 min): 23124.D (-) m/z 149.’9(3 100.00% 1$0

5000 115 52 78 11.40 11.60 11.80 12.00 ........ ... 40 4t ..................... ....... m/z 151.90 , 64.71% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichloroben2ene-d4 1!i0

5000 115 ............. I................. 78 11.40 11.60 11.80 12.00 52 m/z 115.00 , 35.35% 35 87 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1.2,3,4-d4-. 5.6-dichloro- 150 T L 115 11.40 11.60 11.80 12,00 5000 52 78 m/z 77.95 22.05% !! 35 87

m/2-> 30 40 50 60 70 's'o 90 " 100 iw 120 130 140 150 160 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- 152 11.40 11.60 11.80 12.00 m/z 52.00 17.70% 106 5000 53 81

92 .......... 122 k 1“^ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.40 11.60 11.80 12.00

23124.D NP091101.M Tue Oct 09 12:37:18 2001 Page 3

NYC-WTC_000088009

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NYC-WTC_000088009Source: NYC Law Department, mirrored locally

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