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GC/MS analysis results for sample AD23124, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23124 conducted on October 12, 2001.

NYC-WTC_000088000–000088022

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088010
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT0401\23124.D Vial: 12 Acq On : 5 Oct 2001 2:18 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L

Peak Number 4 Butyl hexadecanoate Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

29.53 2.87 ug/1 , 584657 Chrysene-dl2 33.16

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butyl hexac^canoate 312 C2 0H40O2: 000000-00-0 35 2 1-Hexene, /-methyl- 98 C7H14 006094-02-6 27 3 1-Penten^ 2,4-dimethyl- 98 C7H14 002213-32-3 27 4 Cyclobut;Zne, 1,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 27 Abundance / Scan 2668 (29.532 min): 23124.D (-) m/z 56.0,0 100.00% 53

5000- 41 73 129 257 312 It _-J?i20_2940_J9,60_ja8^ m/z 57.0,0 44.66% Tl/Z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44549: Butyl hexadecanoate 56

5000 258 312 It TV __29;20_2946_2?JBp_2a8g_^_ 73 129 240 m/z 43.05 39.02% I I 157171 ISO 214 4^ A )m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #63261: l-Hexene, 2-methyl- 56

29.20 29.40 29.60 29.80 41 5000 m/ z 41.05 37.66% 27 70 98 -n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #63263:1-Pentene. 2,4-dimethyl- I ,A 29.20 2940 29'60 29'80 T 5(6 m/z 73.00 31.59% 4 5000 27 70 98 .11 II ■ I ■ ■ . I I I . I'T I . V I I I . 20 40 60 80 i I I I I I I ■ I r. I . I I ■ J I I ■ I I I I I I I . I . , I I r I I I I . . < I 100 120 140 160 180 200 220 240 260 280 300 iX -T-rj 29.20 29.40 29.60 29.80

23124.D NP091101.M Tue Oct 09 12:37:26 2001 Page 4

NYC-WTC_000088010

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NYC-WTC_000088010Source: NYC Law Department, mirrored locally

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