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GC/MS analysis report, sample AD23798, Nov 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23798 showing detection of unknown compounds on November 1, 2001.

NYC-WTC_000089299–000089310

Folder label: “GC/MS Scan 10/1/01

Page image
Scanned page image, NYC-WTC_000089309
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LibraryL_Search_Compound Report

Data File : C:\HPCHEM\1\DATA\OCT3001\23798.D Vial: 9 Acq On : 30 Oct 2001 10:20 pm Operator; 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.54 ug/1’ 139262 1,4-Dichlorobenzene-d4 11.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlorob^zene-d4 150 C6C12D4 003855-82-1 50, 2 Benzene-1,2 ,^4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 16 3 Benzaldehyi , 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 4 IH-Pyrrol^ [2,3-b]pyridine-2,6-dione 152 C7H8N2Q2 017384-56-4 9 Abundance Scan 711 (11.575 min); 23798.D (-) Tm/z 149.90, 100.00% 1!i0

5000 115

52 78 11.20 11.40 11.60 11.80 12.00

TiZz-> 30 tUs ,,,, ,,1L. 40 50 60 '' I ’''' I'''' I' 70 80 , 90 100 110 120 I ' ' ' ' I 130 140 4U- 150 160 m/z 151.90 . 63.74% Abundance #9593; 1,4-Dichlorobenzene-d4 1!i0

5000 115 78 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 17763% 35 ' I ' ' ' ' I ' ' ' I ' ' ' I ' . ....... 1,1,. ........... 30 40 50 60 70 80 90 100 110 120 130 140 150 160 ^bundar #9592:Ben2ene-1,2,3,4-<J4-,-5,6-dichloro- liiO

11'20 11'40 11^60 11.80 12'00 115 5000- 52 78 m/z 78.05 18.96%

---- 87 I ' I'''' I'''' I'''' I'''' I ‘' I' I ' ' ' ' I nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance .#66892; Benzaldehyde, 2-hydroxy-3-methoxy-_ -11r20-11-.40 -11.60-11 80-12.00 m/z 52.00 . 15.58% 106 ___ 5000- 53 81

' I'''' I *''' I 11111' I' I' 11111 92 122 I I ■'■■I I ' '-’■I ' il 136 . I, J n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

23798.D NP103001.M Thu Nov 01 12:05:04 2001 Page 3

NYC-WTC_000089309

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NYC-WTC_000089309Source: NYC Law Department, mirrored locally

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