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GCMS analysis results for sample AD24135, Nov 1 2001

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Laboratory report documenting GCMS analysis of sample AD24135 conducted on November 1, 2001, noting unknown compounds.

NYC-WTC_000067962–000067973

Folder label: “GCMS Scan X 10/9/01 An 10/31/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3001\24135.D Vial: 22 Acq On : 31 Oct 2001 12:25 pm Operator: 209 GALOS San^jle : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.56 ug/1 122979 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-l_jX 3,4-d4-, 5, 6-dichloro- 150 C6C12D4 002199-69-1 25 3 1H-Pyrroi:o [2,3-b]pyridine-2,6-dione 152 C7H8N2O2! 017384-56-4 9 4 Acenaphthylene 152 C12H8 000208-96-8 9 Abundance Scan 711 (11.574 min): 24135.D (-) m/z 149.90 100.00% 1$0

5000 115 78 52 I I . I I . I 1 1 1 r~f I 1 I I I I I I

11.20 11.40 11.60 11.80 12.00 m/z 151.90 66.16% T,Zz~> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 nw

5000 115 ‘ ' I ‘ '

78 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 44.45% 35 J-Xi J mZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3.4-d4-. 5,6-dichlort>- 1!>0

115 1120 11.40 11.60 11.80 12.00 5000 52 78 m/z 77795 23.86%

35 87 I ' I' ‘' I'''' I' ' 1' ‘' I ‘ I ' ' ■ ' I mfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10125:1H-Pyrrolo[2.3-b]pyridine-2.6-dione, 3,3a,4,5-tetra 1!i2 11.20 11.40 11.60 11.80 12.00 109 m/z 52.00 17.82% 53 500) 80 27 67 I 37 124 p-n- m/z-> 20 30 ' I' ‘ ‘' I' 40 50 60 70 80 90 100 110 120 130 140 150 160 TiS'"7L4o"lSotl5o"l2oO

24135.D NP103001.M Thu Nov 01 12:05:55 2001 Page 3

NYC-WTC_000067972

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NYC-WTC_000067972Source: NYC Law Department, mirrored locally

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