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GCMS analysis results for sample AD24135, Nov 1 2001

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Laboratory report documenting GCMS analysis of sample AD24135 conducted on November 1, 2001, noting unknown compounds.

NYC-WTC_000067962–000067973

Folder label: “GCMS Scan X 10/9/01 An 10/31/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3001\24135.D Vial: 22 Acq On : 31 Oct 2001 12:25 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 7.70 0.55 ug/1 121889 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 intative ID MW MolForm CAS# Qual 1 2-Pentano^, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 40 2 Oxirane,/[ (1 -methylethoxy)methyl] - 116 C6H12O2 004016-14-2 36 3 Morpho zine, 4-methyl- 101 C5H11N0 000109-02-4 9 4 Acetayf de 59 C2H5NO 000060-35-5 9 Mxindance Scan 289 (7.700 tnin): 24135.D (-) m/z 42.95 100.00% 4)3

59 5000 101 ■ ' ' I ' ' ' ' I ' ' '' I ' 7.40 7.60 7.80 8.00 .............. ?S||. .... 56.26% TiZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- <113

5000 ' 7.^‘ 7.60 7.80 's.oo' 59 m/z 100.95 23.57% 27 101 83 I...... . I" " I" ‘' 1 ‘' I' I" " I Tife-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 Mxindance #3238; Oxirane, [(l-methylethoxy)methyl]- 4(3 59 7.40 7.60 7.80 ' 8.66''' 5000 Wz 57795 15.76% 31

73 101 t I •pTTTTTTrrprlTTTTTTT nfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 Mxindance #63448: Morpholine, 4-methyl- ----- I',,' I 43 7.40 7.60 7.80 8.00 “m/z 41.05 7.70% 5000

101 71 56 I 82 87 93 i+W+r I"" 111" I ■ ■" I'' • • I “ “ I r nZz-> 20 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 7.40 7.60 7.80 8.00

24135.D NP103001.M Thu Nov 01 12:05:53 2001 Page 2

NYC-WTC_000067971

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NYC-WTC_000067971Source: NYC Law Department, mirrored locally

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