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GCMS analysis results for sample AD24487, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24487 conducted on November 13, 2001, identifying unknown compounds.

NYC-WTC_000068572–000068584

Folder label: “508 Scan X 10/16/01 A 11/5/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0501\24487.D Vial: 5 Acq On : 5 Nov 2001 3:51 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L A******************************************************************** Peak Number 3 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 1.82 ug/1 300023 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 38 2 Butane yZ 58 C4H10 000106-97-8 9 3 MorphoZine, 4-methyl- 101 C5H11NO 000109-02-4 9 4 3-Hy^oxy-2-pentanone____________ 102 C5H10O2 003142-66-3 9 Abundance Scan 288 (7.686 min): 24487.D (-) m/z 42.95 100.00% 4(3

5000 59

101 7.40 7.60 7.80" 8.00 83 59.05 ' I ' ' ' ' I ' ' I I I ■ ‘ ■ 1 ' ra/z 48.25%

J tt/z-> 10 20 30 40 50 7060 80 90 100 110 Abundance #64275:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 7.40 7.60 7.80 8.00 m/z 100.95 22.53% 15 31 101 -r-i-I-T-iir-r-r-r-i-rJ-r-J-r ' I ' ' I ' I ' ' ' ' I ' ' ' ' I ' ' ' ‘ I n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62336: Butane 43 i . __Z40_760__780_a00__ 5000 29 m/z 58.05 16.63%

-n/z-> Abundance 10 15

20 30 40 50 58 '' I I ' ' ' ' I ' ’ ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' 60 #1640: Morpholine. 4-methyl- 4|3 70 80 90 100 110

m/z 7.40 7.60 41.05 LT 7.80 8.00 7.18%

5000 101 15 71 ,,,l.... I 58 .... ........................ 4 ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' 7.^ ' ' 7.60 ' ' Z80 ' 8.00 ■nfe-> 10 20 30 40 50 60 70 80 90 100 110

24487.D NP103001.M Fri Nov 09 12:00:42 2001 Page 3

NYC-WTC_000068582

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NYC-WTC_000068582Source: NYC Law Department, mirrored locally

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