Laboratory report documenting GCMS analysis of sample AD24491 conducted on November 13, 2001, identifying unknown compounds.
NYC-WTC_000068622–000068633Folder label: “508 Scan X 10/16/01 A 11/5/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0501\24491.D Vial: 10 Acq On : 5 Nov 2001 8:45 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.70 1.02 ug/1 184504 1,4-Dichlorobenzene-d4 11.71
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Pentanone, y4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 56 2 3 - Hydroxy - 2/^ en t anone 102 C5H10O2 003142-66-3 9 3 Morpholin^ 4-methyl- 101 C5H11NO 000109-02-4 9 4 CH2=CHCH^(O)OCH3___________ 100 C5H8O2 003724-55-8 9 Abundance Scan 289 (7.700 min): 24491 .D (-) m/z 42.95 100.00% 40
5000
T)^-> . ...................................... 10 20 30 40 49 ' ' ' I ' ''I 50 60 59
II.......................... 70 80 90 100 I....,110 101 ' ' I ' ‘ 7.40 m/z ' I ' 7.60 59.05 L 7.80 8.00 47.61% ^bundance #64274: 2-Pentanone, 4-hydroxy-4-methyl-
JL 4)3
5000 59 7.40 7.60 7.80 8.00
27 101 I I —tH—T-T—[— I J' ' ' ' I r Tife-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1691:3-Hydroxy-2-pentanone 3|1 59
7.40 7.60 7.80 8.00 5000 m/z 58.05 16.41% 45 15 I ' I ‘ ' I 66 73 84 I I ' ' ' ' I ''' ' ' I ' ' ' ‘ 1 ' ‘ 102 ' I ' ' ' ' 1 mfe-> 10 20 30 40 50 60 70 80 90 100 110
u Abundance #1640: Morpholine, 4-methyl- 4(3 7.40 7.60 7.80 8.00 m/z 41.00 5.65%
5000 101 15 71
I ‘ I ' I ' 27 56 r+Tyn i-fL-i—TT—|—1—r-rT-T-TT-r-r-fA-T-T-T^
10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00
24491.D NP103001.M Fri Nov 09 12:27:29 2001 Page 2
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NYC-WTC_000068598
Laboratory report documenting GCMS analysis of sample AD24489 conducted on November 13, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068684
Laboratory report documenting GCMS analysis of sample AD24642 with detection of unknown compounds on November 13, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068907
Laboratory report documenting GCMS analysis of sample AD24731 identifying unknown compounds on November 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068696
Laboratory report documenting GCMS analysis of sample AD24694 with detection of unknown compounds on November 13, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068672
Laboratory report documenting GCMS analysis of sample AD24641 with detection of unknown compounds on November 13, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068610
Laboratory report documenting GCMS analysis of sample AD24490 conducted on November 13, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068708
Laboratory report documenting GCMS analysis of sample AD24695 with detection of unknown compounds on November 13, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068572
Laboratory report documenting GCMS analysis of sample AD24487 conducted on November 13, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068942
Laboratory report documenting GCMS analysis of sample AD24873 identifying unknown compounds on November 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068799
Laboratory report documenting GCMS analysis of sample AD24486 identifying unknown compounds on November 13, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068919
Laboratory report documenting GCMS analysis of sample AD24732 identifying unknown compounds on November 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068967
Laboratory report documenting GCMS analysis of sample AD24875 identifying unknown compounds on November 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000068555
Record of a GCMS scan conducted at the World Trade Center site in mid-November 2001.
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NYC-WTC_000068556
Log sheet recording liquid-liquid extraction parameters and sample processing details for November 2001.
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NYC-WTC_000068559
Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.
Filed in the same folder
NYC-WTC_000068572
Laboratory report documenting GCMS analysis of sample AD24487 conducted on November 13, 2001, identifying unknown compounds.
Filed in the same folder
NYC-WTC_000068585
Laboratory report documenting GCMS analysis of sample AD24488 conducted on November 13, 2001, identifying unknown compounds.
Filed in the same folder