Laboratory report documenting GC/MS analysis of sample AD25073 conducted on November 28, 2001.
NYC-WTC_000069409–000069419Folder label: “GCMS Scan X 10/23/01 An 11/9/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0901\25073.D Vial: 14 Acq On : 10 Nov 2001 1:05 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method ; C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 2.45 ug/1 347318 1,4-Dichlorobenzene-d4 11.71
Hit# of 5 ;ntative ID MW MolForm CAS# Qual
1 2-Pent ano: , 4-hydroxy-4-methy1- 116 C6H12O2 000123-42-2 56 2 Butane / 58 C4H10 000106-97-8 9 3 Morpholiii e, 4-methyl- 101 C5H11N0 000109-02-4 9 4 3-Hydroxy-2-pentanone 102 C5H10O2 003142-66-3 9 Abundance I. Scan 288 (7.685 min): 25073.D {-) m/z 42795 100.00% 4(3
TI^-> 5000
....................................... 3§ I 50 I 59
' ' I ' ' ' ' I ' ' ' ' I ' ' ' 'I' ' ' ' I ' ' I'' I ' ‘ ' I ' ' ' ' I 10 20 30 40 50 60 70 80 83 ' I ' 90 101
I I I I ' ' ' I 100 110 7.40 m/z L 7.60 59705 7.80 8.00 49.53% Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 4(3
5000 ■tttt '■' ' 59 7.40 7.60 7.80 8.00 m/z 100.95 22.13%
L 27 83 l„ ................... j, |l, , , , I I , ,,,,' I ' ' ' ' I ' I ' ' ' I I ' ' ' ' I T,/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62336: Butane 43
7.40 7.60 7.80 8.00 5000 29 m/z 58.05 16.35%
58 15 I I ' ' I ' ' ''' I ' ' ' ' I ' ' ' ' I ' ‘ ' I ' ' ‘ ' I ' ‘ ‘ ' I ■nfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1640: Morpholine, 4-methyl- 4)3 7.40 7.60 7.80 8,00 m/z 41.05 7.25%
5000 101 15 71 I I ' ' ' ' I 27 I 56 I ' I I ' ' I ' ' I ' I ' ' ' ' I ' ' ' ' I ' ' ' ‘ I ' ' ' ' I ' ' ' ' I n/z-* 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00
25073.D NP103001.M Tue Nov 27 11:11:58 2001 Page 2
NYC-WTC_000069418
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NYC-WTC_000069863
Laboratory report documenting GCMS analysis of sample AD25732 conducted on November 29, 2001, noting other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069484
Laboratory report documenting GCMS analysis of sample AD25263 conducted on November 28, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069463
Laboratory report documenting GCMS analysis of sample AD25261 conducted on November 28, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068737
Laboratory report documenting GCMS analysis of sample AD24333 with detection of unknown compounds on November 27, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069918
Laboratory report documenting GCMS analysis of sample AD25737 conducted on November 29, 2001, noting other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069874
Laboratory report documenting GCMS analysis of sample AD25733 conducted on November 29, 2001, noting other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069452
Laboratory report documenting GC/MS analysis of sample AD25260 conducted on November 28, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069885
Laboratory report documenting GCMS analysis of sample AD25734 conducted on November 29, 2001, noting other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068518
Laboratory report documenting GCMS analysis of sample AD24479 conducted on November 14, 2001, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069676
Laboratory report documenting GCMS analysis of sample AD25462 conducted on November 26, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069234
Laboratory report documenting GCMS analysis of sample AD25039 conducted on November 19, 2001, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069291
Laboratory report documenting GC/MS analysis of sample AD25043 conducted on November 27, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000069345
Department of Environmental Protection GCMS scan log entry dated October 23, 2001.
Filed in the same folder
NYC-WTC_000069346
Log sheet recording liquid-liquid extraction parameters and sample processing details for November 2001.
Filed in the same folder
NYC-WTC_000069349
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 8, 2001.
Filed in the same folder
NYC-WTC_000069357
Laboratory report documenting GC/MS analysis of sample AD25049 conducted on November 28, 2001.
Filed in the same folder
NYC-WTC_000069369
Gas chromatography-mass spectrometry analysis report for sample AD25050 identifying other unknown compounds with violation notation.
Filed in the same folder