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GCMS analysis results for sample AD24948, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24948 conducted on November 19, 2001, noting unknown compounds.

NYC-WTC_000069106–000069116

Folder label: “GCMS Scan X 10/18/01 An 11/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0601\24948.D Vial: 16 Acq On : 7 Nov 2001 3:24 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.68 1.48 ug/1 257342 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 'entative ID MW MolForm CAS# Qual 1 2-PentanMe, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 40 2 3-Hydrow-2-pentanone 102 C5H10O2 003142-66-3 9 3 5-Hexe^2-one 98 C6H10O 000109-49-9 9 4 Morplyfline, 4-methyl-______________ 101 C5H11NO 000109-02-4 9 Abundance Scan 288 (7.685 min): 24948.D (-) m/z 42.95 100.00% 4)3

5000 59

101 7.40 7.60 7.80 8.00 53 , m/z 59.05 48.85% ' ' I ' ................. ............... .... nfe-> 10 20 30 40 50 60 70 80 90 100 110 Mjimdance #64274:2-Pentanone, 4-hydroxy-4-methyI- 4|3

ax)o ----- 1 I > I I I . I I I I . I I I . TrT-i I r-r 59 7.40 7.60 7.80 8.tX) m/z 100.95 20.78% 27 101 I I 83 I ........ .. n&-> 'l0 ' ' M ' 3(3 40 50 «) 70 80 90 100 110 Abundance #1691:3-Hydroxy-2-pentanone 31 59 , rr-r 7.40 7.60 7.80 8.00 5000 m/z 58.05 17.30% 45 15 I ' I ‘ ‘ ‘ 1 ‘ ‘ ' I ' ' ■ I ' ‘ ‘ I. 1 ‘ 66 73 ‘ ' 1 ' ■ ' ' I ‘ 84 102 ‘ ' I ' ' ' ‘ I ‘ ' 1 10 20 30 40 50 a) 70 80 90 100 110 'Vbundance #63205:5-Hexen-2-one 4|3 7.40 1.^ 7.80 8.00 m/z 41.05 6.66% 5000

55 38 , 1 I ‘ ‘ 35 ‘ I ' ■ ' ‘ I ' ’ ' ' I ■ ' • H ■ ' • ‘ I ' 1 ‘ • 1 • ' ' ' 1 I nfe-> 10 20 30 40 50 60 70 80 90 100 110 tSotSt^ob^

24948.D NP103001.M Fri Nov 16 15:20:34 2001 Page 1

NYC-WTC_000069114

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NYC-WTC_000069114Source: NYC Law Department, mirrored locally

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