Laboratory report documenting GC/MS analysis of sample AD25051 conducted on November 28, 2001.
NYC-WTC_000069379–000069388Folder label: “GCMS Scan X 10/23/01 An 11/9/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0901\25051.D Vial: 7 Acq On : 9 Nov 2001 6:17 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P
Quant Method : C;\HPCHEM\1\METHODS\NP103001 .M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 2.45 ug/1 378832 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4^zhydroxy-4-methyl- 116 C6H12O2 000123-42-2 39 2 CH2=CHCH2C(OX5cH3 100 C5H8O2 003724-55-8 10 3 3-Hydroxy^^^2^pentanone 102 C5H10O2 003142-66-3 9 4 Morpholine, 4-methyl- 101 C5H11N0 000109-02-4 9 Abundance Scan 288 (7.687 min): 25051 .D (-) m/z 42.95 100.00% 40
59 5000
101 7.40 7.60 7.80 8.00 53 , . . 71 83 ......................... ' I ' ' ■ I' • I ' I ' ' ' ' I ''' ' ' I ’ I I I ' ■ ' I ' m7z 59.05 49771% ■n&-> 10 20 30 40 50 70 60 80 90 100 110 Wjundance #3245:2-Pentanone, 4-hydroxy-4-methyl- 40
5000 59 _7:40_7;6g__A80__8t0__ m/z 101.05 22787% 31 S? 101 I I 73 .1 ' I ' ' ' ' I ' ' ' ‘ 1 ' ' ' ' I ' ' ' ' I ' Tife-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 40
7.40 7.60 7.80 8.00 5000 m/z 58.05 17.83%
58 ' I ' ‘ I 7 19° ' I TT-r-r-T—r-r-j—I—i—r-r-j—n—r-T-(-r-r-r—i—|—, n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1691:3-Hydroxy-2-pentanone 31 59 7.40 7.60 7.80 8.00 m/z 41.00 7.16% 5000 45 15 ...I...... II...... , 66 I p ' I I I ' ' ' 73 84____102 ' I ' ' ' ■ I I ■ ■ I I I I I ■ I I ■nfe-> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00
25051.D NP103001.M Tue Nov 27 11:10:21 2001 Page 1
NYC-WTC_000069387
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NYC-WTC_000069369
Gas chromatography-mass spectrometry analysis report for sample AD25050 identifying other unknown compounds with violation notation.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069474
Laboratory report documenting GCMS analysis of sample AD25262 conducted on November 28, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069614
Laboratory report documenting GCMS analysis of sample AD25458 conducted on November 26, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069389
Laboratory report documenting GC/MS analysis of sample AD25052 conducted on November 28, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069399
Laboratory report documenting GC/MS analysis of sample AD25072 conducted on November 28, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069978
Laboratory report documenting GCMS analysis of sample AD25664 conducted on November 29, 2001, noting other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069842
Laboratory report documenting GCMS analysis of sample AD25664 conducted on November 29, 2001, noting other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069718
Laboratory report documenting GCMS analysis of sample AD25497 conducted on November 26, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069509
Laboratory report documenting GCMS analysis of sample AD25156 conducted on November 28, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069634
Laboratory report documenting GCMS analysis of sample AD25458 conducted on November 26, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069442
Laboratory report documenting GC/MS analysis of sample AD25259 conducted on November 28, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069624
Laboratory report documenting GCMS analysis of sample AD25459 conducted on November 26, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000069345
Department of Environmental Protection GCMS scan log entry dated October 23, 2001.
Filed in the same folder
NYC-WTC_000069346
Log sheet recording liquid-liquid extraction parameters and sample processing details for November 2001.
Filed in the same folder
NYC-WTC_000069349
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 8, 2001.
Filed in the same folder
NYC-WTC_000069357
Laboratory report documenting GC/MS analysis of sample AD25049 conducted on November 28, 2001.
Filed in the same folder
NYC-WTC_000069369
Gas chromatography-mass spectrometry analysis report for sample AD25050 identifying other unknown compounds with violation notation.
Filed in the same folder