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GC/MS analysis report, sample AD23699, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23699 showing detection of unknown compounds on October 17, 2001.

NYC-WTC_000089158–000089170

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089168
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\23699.D Vial: 12 Acq On : 15 Oct 2001 10:57 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS' 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.75 1.48 ug/1 138768 1,4-Dichlorobenzene-d4 11.77

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone,/4-hydroxy- 4-methyl- 116 C6H1202 000123-42-2 33 2 Morpholine,/4-methyl- 101 C5H11NO 000109-02-4 9 3 Oxirane, [Zl-methylethoxy)methyl]- 116 C6H1202 004016-14-2 9 4 CH2=CHCH2(3(O)OCH3 100 C5H8O2 003724-55-8 9 Abundance Scan 296 (7.755 min): 23699.D (-) m/z ■42795 100.00%) 4)3

5000 59

101 I P w, I , Tn-| I I I I I I 7.40 7.60 7.80 8.00 3^ I 51 -W 83 ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' > ' I I ' ' ' • I I ' ' ' ■ I ■ I I ' I I’l I I I I m/z 59.05 49.19% Ti/i-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 4)3

5000 59 _740_76g^_780__a00^^_ m/z 101.05 19.94% 15 31 101 I I I 83 ' ' I ' ' ' r-p—I—r-i—pr -t+ ' '5'0' ' ' ' I ' ' ' ' I ' ' ' ' I '' ' ' I ' ■nZz-> 10 20 30 40 60 70 80 90 100 110 Abundance #1640: Morpholine, 4-methyl- -4l3---------------- --------- —

7.40 7.60 7.80 8.00 5000 m/z 58.05 17.85% 101

Abundance Uux 10 20 30 • I I I) ■ • I ■ ■ 56I ' I ' 40 50 60 4. 71

70 #64267: Oxirane. [(1-methylethoxy)methyl]- , j",",","7~j~7T::7.7r|l, 7~~~ 80’ 90 100 110 __ 4)3____ ____ ___ — 7:40—7.60 - ---7.80:-- 8.00 ------- 59------ -m/z—4r705 8r09%

5000 . 27 101 73 I _J __ 86 I'''' I' r ''' I ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ■nZz-> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00

23699.D NP091101.M Tue Oct 16 15:10:59 2001 Page 3

NYC-WTC_000089168

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NYC-WTC_000089168Source: NYC Law Department, mirrored locally

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