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GC/MS analysis report, sample AD23656, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23656 showing detection of unknown compounds on October 16, 2001.

NYC-WTC_000089115–000089129

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089127
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\23656.D Vial: 9 Acq On : 15 Oct 2001 8:01 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L A*******************************************************************'* Peak Number 5 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.75 2.15 ug/1 202399 1,4-Dichlorobenzene-d4 11.77

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 2-Pentan(^e, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 28 2 3-Hydros-2-pentanone 102 C5H10O2 003142-66-3 9 3 Morpho^ne, 4-methyl- 101 C5H11NO 000109-02-4 9 4 CH2=5I<CH2C(O)OCH3 100 C5H8O2 003724-55-8 9 Abundance Scan 295 (7.746 min): 23656.D (-) m/z 42.95 100.00% 4b

59 5000

101 ' ' I '' ‘ ' I '' I ' ' ' ' I ' ‘' I ' 7.40 7.60 7.80 8.00 .. ,5.7|.H|., ' I ' ' ' ' I ' I ' ' ' H ' ' ' ' I m/ z 59.05 52.29% 10 20 30 40 50 60 70 80 90 100 110 Abundance #64275:2-Pentanone. 4-hydroxy-4-methyk 43

5000 ■p 59 7.40 7.60 7.80 8.00 m/z 100.95 20.52% 15 31 101 I r I 83 "50^ I ' ' ' ' I ' ' ' ' I ‘ ' Ti/z-> 10 20 30 40 60 70 80 90 100 110 Abundance #1691: 3-Hydroxy-2-pentanone 31’ 59

■7.40 7.60 7.80 8.00 5000- m/z 58.05 14.89% 45

----- ------151- Tl/z-> 10 20 30 40 ' ' '5'0'. ' 60' ' 70 ' ' 'so' '90' ' '160 '110 Abundance #1640: Morpholine, 4-methyl------------- —.43-^----- —----- - ----------------------- I—~ —I.' '...i.ti-' * ' 7.60 / .'7.80 -. 8.00 -.- m/ z 41.00 7.76%

5000 101 15

Tl/Z-> ,,,|. 7, 10 20 30 I 56 71 I ■ I I I I I I > ' I ' I ' ' ' ' I I ' ' ' I I I ' ' I I ; I • I I I ' ' I 40 50 60 70 80 90 100 110 V'Vy'vASA.TV.yTS.z.A/

7.40 7.60 7.80 8.00 P

23656.D NP091101.M Tue Oct 16 15:07:30 2001 Page 5

NYC-WTC_000089127

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NYC-WTC_000089127Source: NYC Law Department, mirrored locally

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