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GC/MS analysis results for sample AD23835, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23835 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089501–000089516

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089513
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File ; C:\HPCHEM\1\DATA\OGT3001\23835.D Vial: 20 Acq On : 31 Oct 2001 9:02 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise . Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ; ************************************************ * * * ****************** Peak Number 5 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. .. ■ J*

7.70 1.03 ug/1 156572 1,4-Dichlorobenzene-d4 11.72

Hit# Of 5 Tentative ID MW MolEbrm CAS# Qual

1 2-Pentanone-hydroxy-4-methy1- 116 C6H12O2 000123-42-2 39 2 3-Hydroxy-^2r-pentanone 102 G5H10O2 003142-66-3 9 . 3 Morpholihe, 4-methyl- 101 C5H11N0 000109-02-4 9 4 4 - Hydrp^ - 3 - hexanone__________________ 116 C6H12d2 004984-85-4 9 Abundance ./ Scan 290 (7.704 min): 23835. D (-) m/z42.95 100.00% 4(3

59 5000

101 ... J ' '' ........ . . . 111 111 I 7.40 7.60 7.80 8.00 .......... 3q I 71 83 ' I ' ' ' ' I ''' ' ' I ' ' ' ' I I . . . I m/z 59.05 52.52% I ' ' ' ' I ' ' ' ' I ' ' ' ‘ I 10 20 30 40 50 60 70 80 90 100 110 Abundance #3245; 2-Pentanone, 4-hydroxy-4-methyl- 4(3

5000 59 - - 7.40 7.60 7.80 8.00 m/z, 101.05 22.29%

iVz-> 10 31 .. ......................... 20 30 40 50 . ......... T,;-' 60 70 80 90 100 110- A Abundance #1691: 3-Hydroxy-2-pentanone 31 ' ' I ' ‘ ' I ' ' 7.40 7.60 7.80 8.00 5000 m/z 58.05 18.55% 45 15 ; “66““73---- 84“^ ' “102“?*^ ' I ' ' ' ' I ' ' ' ' I I I ' ' • ' I ' ' ' I I I I I ■ 1 I Tife-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1640: Morpholine,'4-methyl- -4t3r-^-------- -.--7:40—7.60—7.80. m/z 41.00 8.29%

5000

101. 71 ;

■ ' M ' ' ' ' I ' ' ' ' I ' ' ‘ ' I ' ' 10 20 30 40 50 60 70 80 90 100 110 : 7.40 7.60 7.80 8.00

23835.D NP103001.M Thu Nov 01 13:23:29 2001 Page 5

NYC-WTC_000089513

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NYC-WTC_000089513Source: NYC Law Department, mirrored locally

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