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GC/MS analysis report, sample AD23656, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23656 showing detection of unknown compounds on October 16, 2001.

NYC-WTC_000089115–000089129

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089126
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\23656.D Vial: 9 Acq On : 15 Oct 2001 8:01 pm Operator: 2 09 GALOS; Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE. Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 6.74 0.55 ug/1 51794 1,4-Dichlorobenzene-d4 11.77 Hit# Of 5 Tentative ID MW MolForm CAS# Qua!' 1 2-Hexanol 102 C6H14O 000626-93-7 83- - 2 2-Pentzanol, 4-methyl- 102 C6H14O 000108-11-2 83 . 3 2-Butanol 74 C4H1O0 000078-92-2 50. 4 2-H/canol, (R) -________________________ 102 C6H14O 026549-24-6 43 Abundance/ Scan 185 (6.736 min): 23656.D (-) in/z 44.95 100.00% 4b

TiZz-> 5000

Abundance 10 15 I''' ’ I'''' I'''' I 41 56 69 I 73 +441-Vr..p.^+44^ " I''' 11 " '' I " " I " ' M ' I " I " " I' 20 25 30 35 40 45 50 55 ’ 60 65 70 75 80 85 90 95 #63584:2-Hexanol 8487 6.40 m/z 6.60 6^700 u 6.80 7.00 15.72%

4b

5000 6.40 6.60 6.80 7.00 69 m/z 42.95 13721% 19 SB I 8487 ' I'''' r ''' I' *'' r ''' r ''' H ''' r ''' I''' 11'' r I'''' I'''' r I' * I ‘' I' TiZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95

Jnw Abundance #63547:2-Pentanol, 4-methyl- 4b

6.40 6.60 6.80 7.00 5000 "mTz 41.05 12.23%

27 69 , _ -- ------- 1--- -- “84-87-— ■ I > ( I I I I I I I I I I I I H I I I ( I I I I 1 ■ I I I I I I I I I I I I 1 I I I I

Ti/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance * #334:2-Butanol 7*415=-^ —----- - ^ -6.40—6:60—6M 7.00- ' m/z 43.90 11.11% 5000-

27'31 59 19 55 rTTTTTTTTT+T™r^^+TTTTTTTTTS4++nn-T™^+T+^+TTT^^73 4'I TlZZ-> 10 15 20 25 30 35 40 45 50 55 60 65'' 'vO 75 80 85 6.40 6 60 6 80 7 00

23656.D NP091101.M Tue Oct 16 15:07:28 2001 Page 4;

NYC-WTC_000089126

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NYC-WTC_000089126Source: NYC Law Department, mirrored locally

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