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GCMS analysis results for sample AD24697, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24697 with detection of unknown compounds on November 19, 2001.

NYC-WTC_000068825–000068837

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0501\24696.D Vial: 17 Acq On : 6 Nov 2001 3:34 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L *****************************************************************'**** Peak Number 2 2-Hexanol Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.66 0.40 ug/1 66800 1,4-Dichlorobenzene-d4 11.71 Hit# Of 5 fentative ID MW MolForm CAS# Qual 1 2-Hexanal 102 C6H14O 000626-93-7 78 2 2-Pentanol, 4-methyl- 102 C6H14O 000108-11-2 64 3 2-Butanol 74 C4H10O 000078-92-2 45 4 2-/Pentanol, 3-chloro-4-methyl-, (R@ 136 C6H13C1O 074685-47-5 43 ^bundarfce Scan 176 (6.662 min): 24696. D (-) m/z 44795 100.00%! 4)5

553 --TT-rn-i-rnrrn-p-T-T-T-pr-T-r-r-^^ 69 51 I , 98 6.40 6.60 6.80 7.00 1 “ “ I “ “ 1 *' ” I ‘“ 1 11 Illi [Il upITI [ 1111; I rn 11 M 111 il I fill 11 H 11111 fl 111111111 m/z 69700 15.18% Tife-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63584:2-Hexanol 4)5

KXX) 6.40 6.60 6.80 7.00 69 m/z 41.05 17783% M... .............. II i p-iT4p-rr-rpTT-Tp-ri4yrlT-r^ I ‘ ’' ’! “ “ I nfe-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63545:2-Pentanol, 4-methyl- 4$ VAv' ' ' ' 6.^ " 6.^ " 6.ro " 7.00 5000 m/z 43.05 13.27% 69 27 39 , 57 87

TiZz-> Abundance rW 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 #62568:2-ButanoI 4|5 I ‘" h" I ‘' I" " 1"" I

m/z Al • ‘ ‘ 1 • • • • p ’ • • I ‘ 6.40I 6.60 43.95 6.80 • 1 * *■ 7.00 7.99% 5CX)0

nZz-> ..... f3„,l... X..I 31 J 72 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 I ” 1 '1 I*’' ’ I 6.40 L1 « • • ‘ J * ’ • * 1 ‘ 6,60 6.80 7.00 “

24696.D NP103001«.M Tue Nov 13 12:04:10 2001 Page 2

NYC-WTC_000068834

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NYC-WTC_000068834Source: NYC Law Department, mirrored locally

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