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GCMS analysis results for sample AD24697, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD24697 with detection of unknown compounds on November 19, 2001.

NYC-WTC_000068825–000068837

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0501\24696.D Vial: 17 Acq On 6 Nov 2001 3:34 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.42 0.79 ug/1 129703 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanone 100 C6H12O 000591-78-6 91 2 MethylZlsobutyl Ketone 100 C6H12O 000108-10-1 64 3 Propanal 58 C3H6O 000123-38-6 43 4 2-^'exanone, 4-hydroxy-3-propyl - 158 C9H18O2 062338-17-4 39 Abundance Scan 150 (6.424 min): 24696.D (-) m7z 43.05 100.00% 4(3 1 58 553

71 85 100 6.00 6,20 ' 6.^ " 6,^ aTO ' 53 I TrprTTT^TTTTpTTTTTTTr]^^ m/z 58700 62.35% tVz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1556:2-H8xanone 4(3

58 5000 6,00 6.20 6,40 6.60 6,80 m/z sYTU'S 16.57% 27 71 85 1W I... 11I' “' I “ “ I"'' I" " I" " (" " I" " I TTfe-> 20:^30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 1(» Abundance #63351: Methyl Isobulyl Ketone 40

6,00 6.^ 6.^ 6.m 6,80 5000 “mTz 41.05 15.83% 58 27 85 100 14 'I'"-.......I' TTfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #97: Propanal 23 6,^ " 620 " R40 " 6.60 " RTO'

58 m/z 100.00 10.57% 5000

3? 44 ■ I " " I " " I' ‘ " I Tlfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.00 6.20 6.40 6.60 6.80

24696.D NP103001.M Tue Nov 13 12:04:08 2001 Page 1

NYC-WTC_000068833

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NYC-WTC_000068833Source: NYC Law Department, mirrored locally

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