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GC/MS analysis report for sample AD25737, Nov 2001

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DEP laboratory report documenting GC/MS results for sample AD25737 analyzed on November 29, 2001.

NYC-WTC_000070054–000070064

Folder label: “GCMS Scan X 10/29/01 An 11/7/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV1601\25737.D Vial: 28 Acq On : 17 Nov 2001 5:23 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C;\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.44 0.61 ug/1 124896 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm, CAS# Qual 1 2-Hexanon^ 100 C6H12O 000591-78-6 91 2 2-Hexanone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 56 3 Methyl Lsobutyl Ketone 100 C6H12O 000108-10-1 52 4 0xirane<^-methyl-2- (1-methylethyl) 100 C6H120 072221-03-5 45 Abundance Scan 152 (6.439 min): 25737.D (-) m/z 42.95 100.00% 43

58 5000

Ti/z-> Abundance 20 30 40 ux 50 60 71 -A 70 85 I 80 90 100 #63387:2-Hexanone 100

110 120 130 140 6,0) m/z 6.26' '6.^' '6.66 58.0,5 6.80^ 58.99%

43

58 5000 6^ 6.00 6.40 6.60 6.80 100 "m/z 41.05 16.09% I 71 Ti/z-> ' i' 50 60 70 80 90 100 110 120 130 140 <kbundance #11968:2-Hexanone, 4-hydroxy-3-propyl- 43

58 6.66' 6.^ 6.^' ROT 6.^ 5000 29 “inTz 56.95 14.03%

Ti/z-> 20 ' I ' ' ' ‘ I ‘‘‘'11 30 40 50 X 60 71 ■f 70 I so' go' '166 "ii6’"136 140 MO Abundance #63351: Methyl Isobutyl Ketone 43 6.66 '5.26' '6.^ 6.60 6.80‘ m/z 100.05 12.43% 5000 58

I ‘ I * ' ‘ ‘ I ' 72 85 I 100 I •nfe-> 20 30 40 50 60 70^80^0100riol2o"''^^^ 6.00 6.20 6.40 6.60 6.80

2S737.D NP103001.M Thu Nov 29 11:40:12 2001 Page 1

NYC-WTC_000070062

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NYC-WTC_000070062Source: NYC Law Department, mirrored locally

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