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GCMS analysis results for sample A024874, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample A024874 identifying unknown compounds on November 19, 2001.

NYC-WTC_000068954–000068966

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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Scanned page image, NYC-WTC_000068962
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0501\24874.D Vial: 23 Acq On 6 Nov 2001 10:23 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L A******************************************************************** Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.43 0.65 ug/1 117828 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanone/ 100 C6H12O 000591-78-6 86 2 Methyl Isdbutyl Ketone 100 C6H12O 000108-10-1 58 3 2-HexanizJne, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 56 4 2-Hex^one, 4-hydroxy-5-methyl-3-pr 172 C10H20O2 061141-74-0 45 Abundance/ Scan 151 (6.428 min): 24874.D (-) Tm/z 42.95 100.00% 43

58 5000

6.00 6.20 AJ 6.40 6.60 6.80

TTfe-> I.,....,, 20 30 ”404 4JX 50 60 70 80 90 100 110 120 130 140 ■STz 58.05 55793% <Mjundance #1556:2-Hexanone 43

58 5000 6.00 6.20 6.40 6.60 6.80 “mTz 41.05 16747% 27 71 85 100 ,, ,7,ii TT' I I'' ‘' 1'' ‘' 1' ‘ ‘' I ' nfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #63351: Methyl Isobutyl Ketone 43

6.bb' 'e.^' 'e.^' 6.60 'iso' 5000 "m/z 57.00 15.65% 58 27

TiZz-> 20 ULJ 30 40 Yr 50 60 85 100 .7?...,..I................................. ,,,,,,, 70 80 90 100 110 120 130 140 ^bundance #11968:2-Hexanone, 4-hydroxy-3-propyl- 43 6.00 6.20 6.40 6.60 6.80 m/z 100.05 1^/77%

L 58 5000 29

■’I ■■■■!» ... ,1I ‘ 71 I ‘ 1 ‘ ‘ 85 ‘ 1 • ' '' I ' 100 140 mfe-> 30 40 ' sb'' ‘ 60 70 80 90 100 110 1^ 'im' w' 6.00 6.20 6.40 6.60 6.80

24874.D NP103001.M Fri Nov 16 15:37:31 2001 Page 1

NYC-WTC_000068962

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NYC-WTC_000068962Source: NYC Law Department, mirrored locally

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